1: (4-Methylphenyl)-magnesium bromide With copper (I) cyanide in tetrahydrofuran
T=-78 - -20°C; Inert atmosphere;
2: pentafluoropropen-1-yl 4-methylphenyl sulfone in tetrahydrofuran
T=-78°C; 1 h; Inert atmosphere;
3: With ammonium chloride in tetrahydrofuran; water
Cooling with ice;
参考文献
Yamada, Shigeyuki; Shimoji, Kanoko; Takahashi, Toshio; Konno, Tsutomu; Ishihara, Takashi
Chemistry - An Asian Journal, 2010 , vol. 5, # 8 p. 1846 - 1853