1,1,1,3,3,4,4,4-八氟-2-(三氟甲基)-2-丁醇合成路线 （共 7 条）
反应条件
potassium fluoride in acetonitrile
1) -40 to 20 deg C, 9.5 h, 2) 20 deg C, 7 h;
参考文献
Kotun, Stefan P.; Anderson, John D. O.; DesMarteau, Darryl D.
Journal of Organic Chemistry, 1992 , vol. 57, # 4 p. 1124 - 1131
反应条件
hydrogen fluoride; SbF5
T=55°C; 17 h;
参考文献
Kotun, Stefan P.; DesMarteau, Darryl D.
Canadian Journal of Chemistry, 1989 , vol. 67, p. 1724 - 1728
反应条件
bromine(I) fluorosulfate; C5BrF11O
T=-80 - 25°C; 8 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Anderson, John D.O.; DesMarteau, Darryl D.
Journal of Fluorine Chemistry, 1996 , vol. 77, # 2 p. 147 - 152
反应条件
bromine(I) fluorosulfate; C5BrF11O
T=-93 - 25°C; 8 h; Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Anderson, John D.O.; DesMarteau, Darryl D.
Journal of Fluorine Chemistry, 1996 , vol. 77, # 2 p. 147 - 152
反应条件
vinylidene difluoride
T=-80 - 25°C; 8 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Anderson, John D.O.; DesMarteau, Darryl D.
Journal of Fluorine Chemistry, 1996 , vol. 77, # 2 p. 147 - 152
反应条件
T=-80 - 25°C; 8 h; Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Anderson, John D.O.; DesMarteau, Darryl D.
Journal of Fluorine Chemistry, 1996 , vol. 77, # 2 p. 147 - 152
反应条件
T=-93 - 25°C; 8 h; Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Anderson, John D.O.; DesMarteau, Darryl D.
Journal of Fluorine Chemistry, 1996 , vol. 77, # 2 p. 147 - 152
