反应条件
1: 95 percent / SOCl2
2: 98 percent / H2 / Pd/C / ethyl acetate
3: 58 percent / H2 / Rh/Al / acetic acid / 70 h / 58 °C / 2740.88 Torr
4: 80 percent / 1,3,5-trimethyl-benzene / 165 °C
5: 98 percent / LAH / tetrahydrofuran / Heating
6: 96 percent / PDC / CH2Cl2
View Scheme
参考文献
Gong, Leyi; Hogg, J. Heather; Collier, James; Wilhelm, Robert S.; Soderberg, Carol
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 20 p. 3597 - 3600