N,N-二甲基-3-硝基苯胺合成路线 (共 92 条)
反应条件
1,3-dimethyl-imidazolidin-2-one; sodium trimethylsilanethiolate
T=185°C; 24 h;
参考文献
Hwu, Jih Ru; Wong, Fung Fuh; Shiao, Min-Jen
Journal of Organic Chemistry, 1992 , vol. 57, # 19 p. 5254 - 5255
反应条件
potassium isopropoxide in isopropyl alcohol
T=75°C;
参考文献
Prato, Maurizio; Quintily, Ugo; Scorrano, Gianfranco
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 1419 - 1424
参考文献
Braude et al.
Journal of the Chemical Society, 1954 , p. 3586,3593
参考文献
Groll
Chemische Berichte, 1886 , vol. 19, p. 199
参考文献
Forster; Coulson
Journal of the Chemical Society, 1922 , vol. 121, p. 1995
参考文献
Ephraim; Hochuli
Chemische Berichte, 1915 , vol. 48, p. 633
Show Details
Forster; Coulson
Journal of the Chemical Society, 1922 , vol. 121, p. 1995
反应条件
1: 84 percent / HCl, Fe, H2 / ethanol; H2O / 1 h / Heating
2: 93 percent / acetic acid / 0.5 h / 60 °C
View Scheme
参考文献
Jaubert
Bulletin de la Societe Chimique de France, 1899 , vol. <3>21, p. 20
反应条件
potassium hydroxide in dimethyl sulfoxide
1 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Makosza, Mieczyslaw; Golinski, Jerzy; Baran, Janusz
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1488 - 1494
反应条件
potassium hydroxide in dimethyl sulfoxide
1 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Makosza, Mieczyslaw; Golinski, Jerzy; Baran, Janusz
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1488 - 1494
参考文献
Martynoff
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1948 , vol. 227, p. 1371
Bulletin de la Societe Chimique de France, 1951 , p. 214,219