反应条件
1: thionyl chloride / dichloromethane; N,N-dimethyl-formamide / 3 h / 60 °C / |Inert atmosphere; |Schlenk technique 2: triethylamine / diethyl ether; methanol / 1 h / 20 °C / |Inert atmosphere; |Schlenk technique View Scheme
参考文献
Tang, Qiuzheng; Xia, Dexin; Jin, Xiqing; Zhang, Qing; Sun, Xiao-Qiang; Wang, Congyang
Journal of the American Chemical Society, 2013 , vol. 135, # 12 p. 4628 - 4631