alpha,alpha-二溴-4-硝基甲苯合成路线 （共 28 条）
反应条件
sodium hydroxide; bromine in tetrachloromethane; water
参考文献
E. I. Du Pont de Nemours and Company
Patent: US3993704 A1, 1976 ;
反应条件
sodium tetrahydroborate in ethylene glycol dimethyl ether; water T=20°C; 1 h;
参考文献
WO2010/52536 A1, ;
Example 4 ;
参考文献
Wachendorff
Justus Liebigs Annalen der Chemie, 1877 , vol. 185, p. 281
反应条件
N-bromosuccinmide; dibenzoyl peroxide in carbonic acid diethyl ester
1.5 h; RefluxMicrowave irradiation;
参考文献
Pingali, Subramanya R. K.; Upadhyay, Sunil K.; Jursic, Branko S
Green Chemistry, 2011 , vol. 13, # 4 p. 928 - 933
反应条件
N-bromosuccinmide in acetonitrile
T=60°C; 0.833333 h; Flow reactorIrradiation; TimeTemperature;
参考文献
Cantillo, David; De Frutos, Oscar; Rincon, Juan A.; Mateos, Carlos; Oliver Kappe
Journal of Organic Chemistry, 2014 , vol. 79, # 1 p. 223 - 229
反应条件
potassium tert-butylate in tetrahydrofuran; N,N-dimethyl-formamide
T=-73 - -68°C; 0.0166667 h;
参考文献
Makosza, M.; Owczarczyk, Z.
Journal of Organic Chemistry, 1989 , vol. 54, # 21 p. 5094 - 5100
反应条件
2,4,4,6-tetrabromo-2,5-cyclohexadien-1-one; triphenylphosphine in benzene
36 h; Heating;
参考文献
Matveeva; Feshin; Zefirov
Russian Journal of Organic Chemistry, 2001 , vol. 37, # 1 p. 52 - 55
反应条件
dipotassium peroxodisulfate; lithium bromide in acetic acid
T=113°C; 6 h;
参考文献
Citterio, Attilio; Santi, Roberto; Pagani, Anselmo
Journal of Organic Chemistry, 1987 , vol. 52, # 22 p. 4925 - 4927
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in benzene
8 h; Irradiation;
参考文献
Mataka, Shuntaro; Liu, Guo-Bin; Sawada, Tsuyoshi; Kurisu, Masayoshi; Tashiro, Masashi
Bulletin of the Chemical Society of Japan, 1994 , vol. 67, # 4 p. 1113 - 1119
反应条件
bromine
T=195 - 200°C;
参考文献
Freeman,D.J. et al.
Australian Journal of Chemistry, 1978 , vol. 31, p. 2477 - 2490
