4-溴甲基-5H-呋喃-2-酮合成路线 (共 15 条)
反应条件
sodium hydroxide in water T=20°C; 12 h;
参考文献
Crotti, Antonio E. M.; Bronze-Uhle, Erika S.; Nascimento, Paulo G. B. D.; Donate, Paulo M.; Galembeck, Sergio E.; Vessecchi, Ricardo; Lopes, Norberto P.
Journal of Mass Spectrometry, 2009 , vol. 44, # 12 p. 1733 - 1741
反应条件
copper(ll) bromide in water; acetonitrile T=85°C; 10 h;
参考文献
Huang, Xian; Zhou, Hongwei
Organic Letters, 2002 , vol. 4, # 25 p. 4419 - 4422
反应条件
copper(ll) bromide in water; acetonitrile T=85°C; 10 h;
参考文献
Huang, Xian; Zhou, Hongwei
Organic Letters, 2002 , vol. 4, # 25 p. 4419 - 4422
反应条件
carbon tetrabromide; triphenylphosphine in acetonitrile T=25°C; Appel Halogenation; 1 h; Inert atmosphere;
参考文献
Fort, Diego A.; Woltering, Thomas J.; Alker, Andre M.; Bach, Thorsten
Heterocycles, 2014 , vol. 88, # 2 p. 1079 - 1100
反应条件
1: NBS / CCl4 2: NaOH / H2O / Ambient temperature View Scheme
参考文献
Journal of the American Chemical Society, , vol. 102, # 23 p. 7146 - 7149
反应条件
1.1: 89 percent / Zn; AcOH 2.1: 79 percent / NBS; AIBN / CCl4 3.1: BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C 3.2: 70 percent / tetrahydrofuran; hexane / 1 h / -78 °C 4.1: 71 percent / DBU / tetrahydrofuran / 5 h / 20 °C View Scheme
参考文献
Synthesis, , # 17 p. 2813 - 2820
参考文献
Jeon, Hye-Sun; Yeo, Jung Eun; Jeong, Young Cheol; Koo, Sangho
Synthesis, 2004 , # 17 p. 2813 - 2820
反应条件
sodium tetrahydroborate; nickel dichloride in methanol T=0°C; 0.5 h;
参考文献
Tetrahedron, , vol. 50, # 23 p. 6839 - 6858
参考文献
Boeckman, Robert K.; Ko, Soo Sung
Journal of the American Chemical Society, 1982 , vol. 104, # 4 p. 1033 - 1041
反应条件
18-crown-6 ether; potassium chloride in acetonitrile T=40°C; 96 h;
参考文献
Tetrahedron, , vol. 50, # 23 p. 6839 - 6858