1: (2-Bromo-phenyl)-eth-(Z)-ylidene-amine With potassium hexamethylsilazane in tetrahydrofuran; toluene
T=-78°C; 1.5 h;
2: chloro-trimethyl-silane in tetrahydrofuran; toluene
T=-78°C;
参考文献
STATE OF OREGON ACTING BY and THROUGH THE ST. BOARD OF HIGHER EDUCATION ON BEHALF OF THE UNIVERSITY OF OREGON; UNIVERSITY DISPLAY CORPORATION; LIU, Shih-Yuan; XU, Senmiao; KWONG, Raymond, C.
Patent: WO2014/4985 A1, 2014 ;
Location in patent: Page/Page column 57; 58 ;
Abakarov, G. M.; Gasanov, Sh. S.; Maksimenko, A. A.; Vagabov, M.-Z. V.; Sadekov, I. D.
J. Gen. Chem. USSR (Engl. Transl.), 1992 , vol. 62, # 8 p. 1854 - 1858,1525 - 1528
1.1: 85 °C
2.1: potassium hexamethylsilazane / toluene; tetrahydrofuran / 1.5 h / -78 °C
2.2: -78 °C
View Scheme
参考文献
STATE OF OREGON ACTING BY and THROUGH THE ST. BOARD OF HIGHER EDUCATION ON BEHALF OF THE UNIVERSITY OF OREGON; UNIVERSITY DISPLAY CORPORATION; LIU, Shih-Yuan; XU, Senmiao; KWONG, Raymond, C.
Patent: WO2014/4985 A1, 2014 ;
1.1: toluene / 4 h / 110 °C
2.1: 85 °C
3.1: potassium hexamethylsilazane / toluene; tetrahydrofuran / 1.5 h / -78 °C
3.2: -78 °C
View Scheme
参考文献
STATE OF OREGON ACTING BY and THROUGH THE ST. BOARD OF HIGHER EDUCATION ON BEHALF OF THE UNIVERSITY OF OREGON; UNIVERSITY DISPLAY CORPORATION; LIU, Shih-Yuan; XU, Senmiao; KWONG, Raymond, C.
Patent: WO2014/4985 A1, 2014 ;
