2-甲氧基-5-硝基苯乙酮合成路线 （共 6 条）
反应条件
AlCl3, aluminium chloride in dichloromethane T=-5 - 25°C;
参考文献
Du, Zhen-Ting; Lu, Jing; Yu, Hong-Rui; Xu, Yan; Li, An-Pai
Journal of Chemical Research, 2010 , # 4 p. 222 - 227
反应条件
1: diethyl malonate With triethylamine; magnesium chloride in toluene
T=0 - 20°C; 1 h;
2: 2-methoxy-5-nitrobenzoyl chloride in toluene
T=0°C; 0.5 h;
参考文献
F2G LTD
Patent: WO2006/123145 A1, 2006 ;
Location in patent: Page/Page column 62 ;
反应条件
potassium carbonate in acetone
T=20°C;
参考文献
Zhong, Zhenlin; Snowden, Timothy S.; Best, Michael D.; Anslyn, Eric V.
Journal of the American Chemical Society, 2004 , vol. 126, # 11 p. 3488 - 3495
参考文献
Asahi Kasei Kogyo Kabushiki Kaisha
Patent: US6037362 A1, 2000 ;
反应条件
potassium carbonate; acetone
参考文献
Thanawalla et al.
Journal of the Indian Chemical Society, 1959 , vol. 36, p. 674
反应条件
(i) Et2O, (ii) (hydrolysis), (iii) (decarboxylation); Multistep reaction;
参考文献
Newkome,G.R.; Fishel,D.L.
Journal of Organic Chemistry, 1966 , vol. 31, p. 677 - 681
