2-氨基-3,4,5-三甲氧基苯甲酸合成路线 (共 18 条)
参考文献
Arisawa, Mitsuhiro; Theeraladanon, Chumpol; Nishida, Atsushi; Nakagawa, Masako
Tetrahedron Letters, 2001 , vol. 42, # 45 p. 8029 - 8033
反应条件
diazomethane; diethyl ether
参考文献
Mayer; Fikentscher
Chemische Berichte, 1956 , vol. 89, p. 511,517
参考文献
Arai, Kunizo; Shimizu, Sakae; Yamamoto, Yuzuru
Chemical & Pharmaceutical Bulletin, 1981 , vol. 29, # 4 p. 1005 - 1012
反应条件
1: 2 h / 170 °C 2: POCl3, dimethylaniline / toluene / 4 h / Heating View Scheme
参考文献
Gazit, Aviv; Chen, Jeffrey; Harald, App; McMahon, Gerald; Hirth, Peter; Chen, Irit; Levitzki, Alexander
Bioorganic and Medicinal Chemistry, 1996 , vol. 4, # 8 p. 1203 - 1207
反应条件
1: Cyclization; 2: With trichlorophosphate Substitution; 3 h; Heating;
参考文献
Myers, Michael R.; Setzer, Natalie N.; Spada, Alfred P.; Zulli, Allison L.; Hsu, Chin-Yi J.; Zilberstein, Asher; Johnson, Susan E.; Hook, Linda E.; Jacoski, Mary V.
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 4 p. 417 - 420
反应条件
T=150°C; Niementowski reaction; microwave-assisted; 0.666667 h; microwave irradiation;
参考文献
Alexandre, Francois-Rene; Berecibar, Amaya; Besson, Thierry
Tetrahedron Letters, 2002 , vol. 43, # 21 p. 3911 - 3913
反应条件
1: H2O / 0 - 5 °C / pH 6.8-7.3 2: 99.5 percent / 50percent aq. NaOH / H2O / 3 h / 55 - 57 °C / pH > 13 View Scheme
参考文献
Hammen; Allen
Journal of Heterocyclic Chemistry, 1987 , vol. 24, # 6 p. 1701 - 1703
参考文献
Lions
Journal and Proceedings of the Royal Society of New South Wales, 1929 , vol. 63, p. 168,170