hydrogen sulfide in neat (no solvent)
condensation of excess of H2S onto Ge-compd. (-196°C), warming toroom temp., standing for 60 min; fractional low-temp. distn. (collection at -196°C);
参考文献
Drake,J.E. et al.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1976 , p. 366 - 371
Drake, J. E.; Glavincevski, B. M.; Henderson, H. E.; Hemmings, R. T.
Canadian Journal of Chemistry, 1978 , vol. 56, p. 465 - 472
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Gmelin Handbook: S: SVol.4a/b, 1.3.12, page 303 - 305
