1-哌啶 羧酸-3-氧代-甲酯合成路线 （共 5 条）
反应条件
hydrogen; platinum(IV) oxide in ethanol P=2250.2 Torr;
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 35, # 4 p. 289 - 294
反应条件
1: 84 percent / p-toluenesulfonic acid / 0.5 h 2: 62 percent / NaIO4, RuO2 / ethyl acetate; H2O / 18 h / Ambient temperature 3: 77 percent / 7 M aq. HCl / ethanol / 12 h / Heating View Scheme
参考文献
Matsumura; Takeshima; Okita
Bulletin of the Chemical Society of Japan, 1994 , vol. 67, # 1 p. 304 - 306
反应条件
oxalyl dichloride; TEA; dimethyl sulfoxide in dichloromethane
T=20°C; Swern oxidation; 2 h;
参考文献
Smith, Nicole D.; Hayashida, Joji; Rawal, Viresh H.
Organic Letters, 2005 , vol. 7, # 20 p. 4309 - 4312
反应条件
triethylamine in chloroform
T=0 - 20°C; 1 h;
参考文献
Schering Corporation
Patent: US2008/4287 A1, 2008 ;
Location in patent: Page/Page column 64 ;
反应条件
potassium acetate; sodium carbonate
1.) electrolysis, electrochemical oxidation; Yield given. Multistep reaction;
参考文献
Matsumura; Takeshima; Okita
Bulletin of the Chemical Society of Japan, 1994 , vol. 67, # 1 p. 304 - 306
