3-氧代哌啶-1-羧酸乙酯合成路线 （共 17 条）
反应条件
1: benzene / 2 h / Heating
2: 73 percent / NaBH4 / ethanol / Ambient temperature
3: 80 percent / 1M TiCl4, Et3SiH / CH2Cl2
View Scheme
参考文献
Chen Ling-Ching; Wang, Eng-Chi; Lin, Jen-Hom; Wu, Shihn-Sheng
Heterocycles, 1984 , vol. 22, # 12 p. 2769 - 2773
反应条件
1: 67 percent / HCl(g)
2: benzene / 2 h / Heating
3: 73 percent / NaBH4 / ethanol / Ambient temperature
4: 80 percent / 1M TiCl4, Et3SiH / CH2Cl2
View Scheme
参考文献
Chen Ling-Ching; Wang, Eng-Chi; Lin, Jen-Hom; Wu, Shihn-Sheng
Heterocycles, 1984 , vol. 22, # 12 p. 2769 - 2773
反应条件
1: 73 percent / NaBH4 / ethanol / Ambient temperature
2: 80 percent / 1M TiCl4, Et3SiH / CH2Cl2
View Scheme
参考文献
Chen Ling-Ching; Wang, Eng-Chi; Lin, Jen-Hom; Wu, Shihn-Sheng
Heterocycles, 1984 , vol. 22, # 12 p. 2769 - 2773
反应条件
1: 75 percent / K2CO3 / H2O / 3 h / Ambient temperature
2: 73 percent / NaBH4 / ethanol / Ambient temperature
3: 80 percent / 1M TiCl4, Et3SiH / CH2Cl2
View Scheme
参考文献
Chen Ling-Ching; Wang, Eng-Chi; Lin, Jen-Hom; Wu, Shihn-Sheng
Heterocycles, 1984 , vol. 22, # 12 p. 2769 - 2773
反应条件
hydrogenchloride
20 h; Heating; Yield given;
参考文献
Garst, Michael E.; Bonfiglio, John N.; Grudoski, David A.; Marks, Jeffrey
Journal of Organic Chemistry, 1980 , vol. 45, # 12 p. 2307 - 2315
反应条件
in benzene
T=25°C; 1 h;
参考文献
Brubaker; Colley Jr.
Journal of Medicinal Chemistry, 1986 , vol. 29, # 8 p. 1528 - 1531
反应条件
toluene-4-sulfonic acid in benzene
Heating; Title compound not separated from byproducts;
参考文献
Takayasu, Tohru; Nitta, Makoto
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 6 p. 687 - 692
