n-甲基-n-2-吡啶乙酰胺合成路线 (共 5 条)
反应条件
(η5-cyclopentadienyl)2TiF2; methylphenylsilane in toluene T=20°C; 0.5 h;
参考文献
Selvakumar, Kumaravel; Rangareddy, Kesamreddy; Harrod, John F.
Canadian Journal of Chemistry, 2004 , vol. 82, # 8 p. 1244 - 1248
反应条件
lithium diisopropyl amide 1.) 3 h, room temperature, 2.) pH 9.2 buffer, overnight; Yield given. Multistep reaction;
参考文献
Barrett, Anthony G. M.; Morris, Timothy M.; Barton, Derek H. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2272 - 2277
参考文献
Okamoto, Iwao; Terashima, Masayuki; Masu, Hyuma; Nabeta, Mayumi; Ono, Kaori; Morita, Nobuyoshi; Katagiri, Kosuke; Azumaya, Isao; Tamura, Osamu
Tetrahedron, 2011 , vol. 67, # 44 p. 8536 - 8543
反应条件
potassium tert-butylate in tetrahydrofuran
12 h; Heating;
参考文献
Barrett, Anthony G. M.; Morris, Timothy M.; Barton, Derek H. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2272 - 2277
反应条件
in dichloromethane
T=0 - 20°C;
参考文献
Manley, Peter J; Bilodeau, Mark T
Organic letters, 2002 , vol. 4, # 18 p. 3127 - 3129