反应条件
1: oxalyl dichloride / dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere 2: pyridine / 1,2-dichloro-ethane / 50 °C / Inert atmosphere View Scheme
参考文献
Sams, Anette G.; Mikkelsen, Gitte K.; Larsen, Mogens; Langgard, Morten; Howells, Mark E.; Schroder, Tenna J.; Brennum, Lise T.; Torup, Lars; Jorgensen, Erling B.; Bundgaard, Christoffer; Kreilgard, Mads; Bang-Andersen, Benny
Journal of Medicinal Chemistry, 2011 , vol. 54, # 3 p. 751 - 764