1.1: hydroxylamine hydrochloride / ethanol / 0.58 h / 20 °C 2.1: hydrogenchloride; zinc / ethanol; water / 0.25 h / 20 °C 2.2: 0.25 h / 20 °C View Scheme
参考文献
Ayedi, Mohamed Ali; Le Bigot, Yves; Ammar, Houcine; Abid, Souhir; Gharbi, Rachid El; Delmas, Michel
Synthetic Communications, 2013 , vol. 43, # 16 p. 2127 - 2133
iodobenzene in N,N-dimethyl-formamide T=5 - 10°C; electrolysis: undivided electrochemical cell, Bu4NBF4 as a supporting electrolyte, sacrificial Mg anode, Ni grid cathode freshly coated with a small deposit of Cd, constant current with density of 1 A dm-2;
参考文献
Barhdadi, Rachid; Troupel, Michel; Perichon, Jacques
Chemical Communications, 1998 , # 12 p. 1251 - 1252
