1.1: 90 percent / aq. CAN / acetonitrile / 20 °C 2.1: HC(OMe)3 / methanol / 20 °C / pH 6 2.2: 74 percent / NaBH4 / methanol / 16 h / 0 °C 3.1: 69 percent / aq. CAN / acetonitrile / 20 °C View Scheme
参考文献
Bull, Steven D.; Davies, Stephen G.; Fenton, Carry; Mulvaney, Andrew W.; Shyam Prasad; Smith, Andrew D.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 22 p. 3765 - 3774
bis(trimethylsilyl)-peroxide; dichlorotriphenylphosphorane in acetonitrile
60 h; Ambient temperature;
参考文献
Shibata, Kazusato; Itoh, Yukinori; Tokitoh, Norihiro; Okazaki, Renji; Inamoto, Naoki
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 12 p. 3749 - 3751
1.1: 90 percent / aq. CAN / acetonitrile / 20 °C
2.1: HC(OMe)3 / methanol / 20 °C / pH 6
2.2: 77 percent / NaBH4 / methanol / 5 h / 0 °C
3.1: 54 percent / aq. CAN / acetonitrile; tetrahydrofuran / 20 °C
View Scheme
参考文献
Bull, Steven D.; Davies, Stephen G.; Fenton, Carry; Mulvaney, Andrew W.; Shyam Prasad; Smith, Andrew D.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 22 p. 3765 - 3774
