4-甲基-N-苯基苯胺合成路线 (共 140 条)
反应条件
sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0) in toluene
参考文献
E. I. du Pont de Nemours and Company
Patent: US6291722 B1, 2001 ;
反应条件
copper diacetate; triethylamine T=20°C; 24 h;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Davan, Elham Etemadi; Rostami, Abed; Nematollahi, Arash
Journal of Organometallic Chemistry, 2013 , vol. 740, p. 123 - 130
反应条件
in dichloromethane T=20°C; 6 h; Molecular sieve;
参考文献
Luo, Jun; Ji, Enwei; Ye, Jingyuan; Wu, Runze; Qiu, Lei
Tetrahedron Letters, 2013 , vol. 54, # 34 p. 4505 - 4508
反应条件
cesium fluoride; bis(dibenzylideneacetone)-palladium(0); 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl T=100°C; 5.5 h; Inert atmosphere;
参考文献
Shimizu, Kenta; Minami, Yasunori; Goto, Osamu; Ikehira, Hideyuki; Hiyama, Tamejiro
Chemistry Letters, 2014 , vol. 43, # 4 p. 438 - 440
反应条件
1,10-phenanthroline; oxygen; palladium diacetate in toluene T=135°C; 37 h; Sealed tube;
参考文献
Girard, Simon A.; Knauber, Thomas; Zhou, Feng; Simon, Marc-Olivier; Li, Chao-Jun; Hu, Xiong; Deng, Guo-Jun
Organic Letters, 2012 , vol. 14, # 21 p. 5606 - 5609,4
反应条件
toluene-4-sulfonic acid T=165°C; 0.75 h; Ionic liquidMicrowave irradiation;
参考文献
Singh, Rahul; Allam, Bharat Kumar; Raghuvanshi, Dushyant Singh; Singh, Krishna Nand
Tetrahedron, 2013 , vol. 69, # 3 p. 1038 - 1042
反应条件
in anhydrous xylene T=140°C; Inert atmosphere;
参考文献
Ou, Lili; Shao, Jiaan; Zhang, Guolin; Yu, Yongping
Tetrahedron Letters, 2011 , vol. 52, # 13 p. 1430 - 1431
反应条件
sodium t-butanolate in toluene
参考文献
E. I. du Pont de Nemours and Company
Patent: US6124462 A1, 2000 ;
反应条件
potassium hydroxide; copper(II) oxide in dimethyl sulfoxide T=110°C; 1.6 h;
参考文献
Rout, Laxmidhar; Jammi, Suribabu; Punniyamurthy
Organic Letters, 2007 , vol. 9, # 17 p. 3397 - 3399
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; [Ni0(1,5-cyclooctadiene)2]; sodium t-butanolate in toluene T=20 - 105°C; Inert atmosphere;
参考文献
Ackermann, Lutz; Sandmann, Rene; Song, Weifeng
Organic Letters, 2011 , vol. 13, # 7 p. 1784 - 1786