4,4'-二甲基二苯胺合成路线 （共 114 条）
反应条件
copper(l) iodide in pyridine 5 h; Heating;
参考文献
Journal of Physical Organic Chemistry, , vol. 7, p. 9 - 17
参考文献
Suzuki, Ken; Kobayashi, Tohru; Nishikawa, Takenobu; Hori, Yoji; Hagiwara, Toshimitsu
Patent: US2002/58837 A1, 2002 ;
反应条件
1: [bis(acetoxy)iodo]benzene / 0.08 h / 25 °C / |Schlenk technique; |Inert atmosphere 2: bismuth trifluoromethanesulphonate / methanol / 25 °C / |Schlenk technique; |Inert atmosphere 3: zinc; trifluoroacetic acid / methanol / 25 °C / |Schlenk technique; |Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 15, # 8 p. 2018 - 2021
反应条件
1: bismuth trifluoromethanesulphonate / methanol / 25 °C / |Schlenk technique; |Inert atmosphere 2: zinc; trifluoroacetic acid / methanol / 25 °C / |Schlenk technique; |Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 15, # 8 p. 2018 - 2021
反应条件
PPA; trifluoroacetic acid in various solvent(s) T=40°C; 3 h; Title compound not separated from byproducts;
参考文献
European Journal of Organic Chemistry, , # 20 p. 3920 - 3922
反应条件
T=600°C; P=0.005 - 0.01 Torr; 0.5 h; Further byproducts given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2200 - 2204
反应条件
trifluoroacetic acid T=85°C;
参考文献
Journal of Organic Chemistry, , vol. 38, # 11 p. 2052 - 2057
反应条件
alpha,alpha-dimethylbenzyl hydroperoxide Arrhenius parameters lg A3 and E3, enthalpie change ΔH3; Thermodynamic dataRate constantEquilibrium constant;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 39, # 4.1 p. 657 - 662
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 4 p. 743 - 749
反应条件
potassium permanganate in water T=95°C; 0.316667 h; microwave irradiation;
参考文献
Synthetic Communications, , vol. 38, # 15 p. 2619 - 2624
反应条件
ammonium chlorozincate; ammonium chloride T=330 - 340°C;
参考文献
Chemische Berichte, , vol. 20, p. 548
