4,4’-二甲基二苯硫醚合成路线 (共 108 条)
反应条件
[bis(acetoxy)iodo]benzene in chloroform T=40°C; Oxidation; 72 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 72, # 10 p. 2351 - 2356
反应条件
oxygen; Titanium(IV) oxide in acetonitrile Irradiation;
参考文献
Tetrahedron Letters, , vol. 31, # 32 p. 4533 - 4536
反应条件
in acetonitrile T=20°C; Irradiation; Title compound not separated from byproducts.;
参考文献
Journal of Organic Chemistry, , vol. 66, # 13 p. 4576 - 4579
反应条件
in benzene 0.5 h; Heating; Product distribution; Further Variations:molar ratios;
参考文献
Tetrahedron Letters, , vol. 46, # 9 p. 1395 - 1397
反应条件
potassium phosphate; copper(l) iodide; potassium thioacyanate in PEG-400
T=150°C; 20 h; Inert atmosphere;
参考文献
Chen, Junmin; Zhang, Yimin; Liu, Li; Yuan, Tangjun; Yi, Fei
Phosphorus, Sulfur and Silicon and the Related Elements, 2012 , vol. 187, # 11 p. 1284 - 1290
反应条件
pyridine; zinc; CoI2(dppe) in acetonitrile
T=80°C; 10 h;
参考文献
Iglesias, Maria Jose; Prieto, Auxiliadora; Nicasioa, M. Carmen
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 11-12 p. 1949 - 1954
反应条件
silver trifluoroacetate; potassium hydroxide in N,N-dimethyl-formamide
T=150°C; 12 h; Molecular sieveInert atmosphere;
参考文献
Das, Rima; Chakraborty, Debashis
Tetrahedron Letters, 2012 , vol. 53, # 52 p. 7023 - 7027
反应条件
potassium phosphate; copper(l) iodide; Na2S*9H2O
T=150°C; 24 h;
参考文献
Chen, Junmin; Zhang, Yimin; Liu, Li; Yuan, Tangjun; Yi, Fei
Phosphorus, Sulfur and Silicon and the Related Elements, 2012 , vol. 187, # 11 p. 1284 - 1290
反应条件
[ReV(O)Cl3(PPh3)2] in chloroform
17 h; Reflux;
参考文献
Sousa, Sara C.A.; Bernardo, Joana R.; Romao, Carlos C.; Fernandes, Ana C.
Tetrahedron, 2012 , vol. 68, # 39 p. 8194 - 8197
反应条件
rhenic(VII) acid in toluene
17 h; Reflux;
参考文献
Sousa, Sara C. A.; Bernardo, Joana R.; Fernandes, Ana C.
Tetrahedron Letters, 2012 , vol. 53, # 46 p. 6205 - 6208,4