4,4’-二甲基二苯硫醚合成路线 （共 108 条）
反应条件
potassium carbonate; zinc; 1,1'-bis-(diphenylphosphino)ferrocene; niobium bromide in N,N-dimethyl-formamide
T=25°C; 10 h; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Takagi, Kentaro
Chemistry Letters, 1987 , p. 2221 - 2224
反应条件
in tetrahydrofuran
T=-50 - 25°C; 0.333333 h;
参考文献
Oae, Shigeru; Akutagawa, Kunihiko; Furukawa, Naomichi
Phosphorus and Sulfur and the Related Elements, 1984 , vol. 19, p. 223 - 234
反应条件
1,10-phenanthroline; CuCl2·2H2O; tetrabutyl ammonium fluoride; potassium thioacyanate; caesium carbonate in water
T=130°C; 48 h;
参考文献
Ke, Fang; Qu, Yanyang; Jiang, Zhaoqiong; Li, Zhengkai; Wu, Di; Zhou, Xiangge
Organic Letters, 2011 , vol. 13, # 3 p. 454 - 457
反应条件
disulfur dichloride; aluminium trichloride
参考文献
Boeeseken; Koning
Recueil des Travaux Chimiques des Pays-Bas, 1911 , vol. 30, p. 128
反应条件
bis(tricyclohexylphosphane)palladium in toluene
T=100°C; 3 h;
参考文献
Osakada, Kohtaro; Yamamoto, Takakazu; Yamamoto, Akio
Tetrahedron Letters, 1987 , vol. 28, # 50 p. 6321 - 6324
反应条件
potassium hydroxide in dimethyl sulfoxide
T=80°C; 38 h; air;
参考文献
Jammi, Suribabu; Sakthivel, Sekarpandi; Rout, Laxmidhar; Mukherjee, Tathagata; Mandai, Santu; Mitra, Raja; Saha, Prasenjit; Punniyamurthy, Tharmalingam
Journal of Organic Chemistry, 2009 , vol. 74, # 5 p. 1971 - 1976
反应条件
toluenethiol; sodium hydride; (10-hydroximino-3,9-dimethyl-4,8-diazaundeca-3,8-dien-2-one oximato)nickel(II) perchlorate
2.) MeCN, irradiation, 6 h;
参考文献
Tada, Masaru; Masuzawa, Yoshihide
Chemical Communications, 1997 , # 22 p. 2161 - 2162
反应条件
methyl-phenyl-thioether; sodium hydride; (10-hydroximino-3,9-dimethyl-4,8-diazaundeca-3,8-dien-2-one oximato)nickel(II) perchlorate
2.) MeCN, irradiation, 6 h;
参考文献
Tada, Masaru; Masuzawa, Yoshihide
Chemical Communications, 1997 , # 22 p. 2161 - 2162
参考文献
Hauptmann; Wladislaw
Journal of the American Chemical Society, 1950 , vol. 72, p. 707
反应条件
sodium hydride; (10-hydroximino-3,9-dimethyl-4,8-diazaundeca-3,8-dien-2-one oximato)nickel(II) perchlorate
2.) MeCN, irradiation, 6 h;
参考文献
Tada, Masaru; Masuzawa, Yoshihide
Chemical Communications, 1997 , # 22 p. 2161 - 2162
