2-乙酰氨基-3,4,6-三-O-乙酰基-2-脱氧-Β-D-吡喃葡萄糖酰基叠氮化物合成路线 （共 23 条）
反应条件
1: 94 percent / Me3SiN3, molecular sieves 3A, SnCl4 / CH2Cl2 / 12 h / Ambient temperature 2: 1.) NaBH4, 2.) pyridine / 1.) CH2Cl2, MeOG, 10 min, 2.) room temperature, 2 h View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 4 p. 405 - 416
反应条件
1: hydrogen bromide / dichloromethane; acetic acid / 5 h / 0 °C 2: tetra-N-butylammonium azide / dichloromethane View Scheme
参考文献
Chemistry - A European Journal, , vol. 19, # 44 p. 14836 - 14851
反应条件
tetra-N-butylammonium azide in dichloromethane
参考文献
Farrell, Mark; Zhou, Jian; Murphy, Paul V.
Chemistry - A European Journal, 2013 , vol. 19, # 44 p. 14836 - 14851
参考文献
Chemische Berichte, , vol. 89, p. 1521,1529
参考文献
Chemische Berichte, , vol. 89, p. 1521,1529
反应条件
pyridine; sodium tetrahydroborate 1.) CH2Cl2, MeOG, 10 min, 2.) room temperature, 2 h; Yield given. Multistep reaction;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 4 p. 405 - 416
反应条件
1: 92 percent / ammonia / methanol / 24 h / Ambient temperature 2: 88 percent / hydrogen / PtO2 (Adam's catalyst) / methanol / 3 h View Scheme
参考文献
Joseph, Ryan; Dyer, Frank Brock; Garner, Philip
Organic Letters, 2013 , vol. 15, # 4 p. 732 - 735
反应条件
hydrogen; palladium on activated charcoal in methanol 0.5 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 36, # 21 p. 3635 - 3638
反应条件
palladium monocarbide in methanol
反应条件
1: sodium methylate; methanol / 2 h / 0 °C 2: human His6-propeptide-placental catβ1,4-galactosyltransferase 1 fusion protein; Campylobacter jejuni UDP-Glc/GlcNAc-4'-epimerase; alkaline phosphatase / |Enzymatic reaction View Scheme
参考文献
Adamiak, Kathrin; Anders, Thorsten; Henze, Manja; Keul, Helmut; Moeller, Martin; Elling, Lothar
Journal of Molecular Catalysis B: Enzymatic, 2012 , vol. 84, p. 108 - 114
