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63148-62-9
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
62051-95-0
合成路线
（共 4 条）
70358-36-0
→
反应条件
62051-95-0
反应条件
hydrogenchloride; sodium nitrite in dichloromethane; N,N-dimethyl acetamide; water; hexan-1-ol T=20°C; 0.02 h; Inert atmosphere;
参考文献
Chen, Mao; Buchwald, Stephen L.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 15 p. 4247 - 4250
Angew. Chem., 2013 , vol. 125, # 15 p. 4341 - 4344,4
5470-18-8
2-氯-3-硝基吡啶
→
反应条件
62051-95-0
反应条件
1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl acetamide; heptan-1-ol / 0.5 h / 170 °C / |Inert atmosphere 2: 5 palladium on charcoal; hydrogen / N,N-dimethyl acetamide; dichloromethane; hexan-1-ol / 45 °C / 258.58 Torr / |Inert atmosphere 3: hydrogenchloride; sodium nitrite / N,N-dimethyl acetamide; dichloromethane; hexan-1-ol; water / 0.02 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Chen, Mao; Buchwald, Stephen L.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 15 p. 4247 - 4250
Angew. Chem., 2013 , vol. 125, # 15 p. 4341 - 4344,4
372-19-0
3-氟苯胺
→
反应条件
62051-95-0
反应条件
1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl acetamide; heptan-1-ol / 0.5 h / 170 °C / |Inert atmosphere 2: 5 palladium on charcoal; hydrogen / N,N-dimethyl acetamide; dichloromethane; hexan-1-ol / 45 °C / 258.58 Torr / |Inert atmosphere 3: hydrogenchloride; sodium nitrite / N,N-dimethyl acetamide; dichloromethane; hexan-1-ol; water / 0.02 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Chen, Mao; Buchwald, Stephen L.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 15 p. 4247 - 4250
Angew. Chem., 2013 , vol. 125, # 15 p. 4341 - 4344,4
14251-84-4
→
反应条件
62051-95-0
反应条件
1: 5 palladium on charcoal; hydrogen / N,N-dimethyl acetamide; dichloromethane; hexan-1-ol / 45 °C / 258.58 Torr / |Inert atmosphere 2: hydrogenchloride; sodium nitrite / N,N-dimethyl acetamide; dichloromethane; hexan-1-ol; water / 0.02 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Chen, Mao; Buchwald, Stephen L.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 15 p. 4247 - 4250
Angew. Chem., 2013 , vol. 125, # 15 p. 4341 - 4344,4
