反应条件
1: 2,7-dibromo-9,9-di-n-octylfluorene With n-butyllithium in diethyl ether; hexane
T=-10°C; 3 h;
2: chloro-trimethyl-silane in diethyl ether; hexane
T=20°C; Further stages.;
参考文献
Jeeva, Shezhad; Moratti, Stephen C.
Synthesis, 2007 , # 21 art. no. P08807SS, p. 3323 - 3328