N,N’-双(对甲苯基)脲合成路线 （共 103 条）
反应条件
tin(IV) chloride; triethylamine; [Pt(triphenylphosphine)2Cl2] in benzene
T=140°C; 4 h;
参考文献
Tsuji, Yasushi; Takeuchi, Ryo; Watanabe, Yoshihisa
Journal of Organometallic Chemistry, 1985 , vol. 290, p. 249 - 256
反应条件
potassium phosphate; 1,2-diamino-cyclohexane; copper(l) iodide in N,N-dimethyl-formamide
T=80°C; 24 h;
参考文献
Nandakumar, Mecheril V.
Tetrahedron Letters, 2004 , vol. 45, # 9 p. 1989 - 1990
反应条件
iodine
T=90 - 95°C; 0.0833333 h;
参考文献
Pasha; Madhusudana Reddy
Synthetic Communications, 2009 , vol. 39, # 16 p. 2928 - 2934
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; caesium carbonate in 1,4-dioxane
T=100°C; 2.5 h;
参考文献
Sergeev, Alexey G.; Artamkina, Galina A.; Beletskaya, Irina P.
Tetrahedron Letters, 2003 , vol. 44, # 25 p. 4719 - 4723
反应条件
tin(IV) chloride; triethylamine; [Pt(triphenylphosphine)2Cl2] in 1,4-dioxane
T=140°C; 4 h;
参考文献
Tsuji, Yasushi; Takeuchi, Ryo; Watanabe, Yoshihisa
Journal of Organometallic Chemistry, 1985 , vol. 290, p. 249 - 256
反应条件
zirconium oxide; molybdenum in 1,2-dichloro-benzene
T=69.85°C; Condensation; 6 h;
参考文献
Reddy, Benjaram M.; Reddy, Vangala R.
Synthetic Communications, 1999 , vol. 29, # 16 p. 2789 - 2794
反应条件
1: in tetrahydrofuran
T=20°C;
2: With 4-(N,N-dimethlyamino)pyridine in tetrahydrofuran
Reflux;
参考文献
Lee, Hyung-Geun; Kim, Min-Jung; Park, Song-Eun; Kim, Jeum-Jong; Kim, Bo Ram; Lee, Sang-Gyeong; Yoon, Yong-Jin
Synlett, 2009 , # 17 p. 2809 - 2814
反应条件
copper acetylacetonate; potassium tert-butylate in 1-methyl-pyrrolidin-2-one
T=20°C; 24 h; Inert atmosphereSealed vial;
参考文献
Gavade, Sandip; Balaskar, Ravi; Mane, Madhav; Pabrekar, Pramod N.; Mane, Dhananjay
Synthetic Communications, 2012 , vol. 42, # 11 p. 1704 - 1714
反应条件
caesium carbonate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in 1,4-dioxane
T=100°C; 20 h;
参考文献
Artamkina, Galina A.; Sergeev, Alexey G.; Beletskaya, Irina P.
Tetrahedron Letters, 2001 , vol. 42, # 26 p. 4381 - 4384
反应条件
sodium azide; [bis(acetoxy)iodo]benzene in acetonitrile
T=0 - 80°C; 36 h; Inert atmosphere;
参考文献
Li, Xiao-Qiang; Wang, Wei-Kun; Han, Yi-Xin; Zhang, Chi
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 14-15 p. 2588 - 2598
