N,N’-双(对甲苯基)脲合成路线 （共 103 条）
反应条件
1: 79 percent / benzene; toluene / 1 h / Ambient temperature
2: 57 percent / TEA / benzene / 22 h / 40 - 50 °C
3: 25 percent / TEA / 20 h / 70 - 80 °C
View Scheme
参考文献
Morkved, Eva H.
Journal fuer Praktische Chemie (Leipzig), 1986 , vol. 328, # 3 p. 393 - 400
反应条件
in methanol; benzene-d6
Kinetics; from 22 to 103°C; monitored by (1)H- and (31)P-NMR;
参考文献
Gargulak, Jerry D.; Gladfelter, Wayne L.
Journal of the American Chemical Society, 1994 , vol. 116, # 9 p. 3792 - 3800
参考文献
Mailhe
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1923 , vol. 176, p. 691
参考文献
Naegeli et al.
Helvetica Chimica Acta, 1938 , vol. 21, p. 1100,1102
Full Text Show Details
Naegeli; Tyabji; Conrad
Helvetica Chimica Acta, 1938 , vol. 21, p. 1127,1139
反应条件
nitrocarbamic acid ethyl ester in 1,4-dioxane
参考文献
Lamberton,A.H. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1974 , p. 956 - 960
反应条件
T=200 - 210°C; 0.75 h;
参考文献
Aly, N. F.; Fahmy, A. F. M.; Baddawy, H. A.; Alkhateeb, A. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 6 p. 489 - 490
反应条件
1: 57 percent / TEA / benzene / 22 h / 40 - 50 °C
2: 25 percent / TEA / 20 h / 70 - 80 °C
View Scheme
参考文献
Morkved, Eva H.
Journal fuer Praktische Chemie (Leipzig), 1986 , vol. 328, # 3 p. 393 - 400
反应条件
dichlorotris(triphenylphosphine)ruthenium(II) in 1,3,5-trimethyl-benzene
12 h; Heating; Title compound not separated from byproducts;
参考文献
Kotachi, Shinji; Tsuji, Yasushi; Kondo, Teruyuki; Watanabe, Yoshihisa
Journal of the Chemical Society, Chemical Communications, 1990 , # 7 p. 549 - 550
反应条件
dodecacarbonyltetrarhodium(0)
T=220°C; 6 h;
参考文献
Mise, Takaya; Hong, Pangbu; Yamazaki, Hiroshi
Chemistry Letters, 1980 , p. 439 - 440
反应条件
tin(IV) chloride; triethylamine; [Pt(triphenylphosphine)2Cl2] in 1,4-dioxane
T=140°C; 4 h; investigated effects of various amines; Product distribution;
参考文献
Tsuji, Yasushi; Takeuchi, Ryo; Watanabe, Yoshihisa
Journal of Organometallic Chemistry, 1985 , vol. 290, p. 249 - 256
