N,N'-二(苯基)丙二酰胺合成路线 (共 79 条)
反应条件
PPA
6 h; 120-140 deg C;
参考文献
Balasubramanian, C.; Kumaraswami, K.; Dharmaraj, N.; Mohan, P. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1993 , vol. 32, # 4 p. 460 - 462
反应条件
disulfur dichloride in benzene
4 h; Heating;
参考文献
Kutney, Gerald W.; Still, Ian W.J.
Canadian Journal of Chemistry, 1980 , vol. 58, p. 1233 - 1238
参考文献
Jolles
Gazzetta Chimica Italiana, 1938 , vol. 68, p. 488,495
反应条件
tetraphosphorus decasulfide; toluene
参考文献
Bakulev, V. A.; Lebedev, A. T.; Dankova, E. F.; Mokrushin, V. S.; Petrosyan, V. S.
Tetrahedron, 1989 , vol. 45, # 23 p. 7329 - 7340
参考文献
Reissert; More
Chemische Berichte, 1906 , vol. 39, p. 3301
反应条件
chlorosulphuric acid
Erwaermen des Reaktionsprodukts mit 2-Amino-aethanol-(1) und wss. Kalilauge;
参考文献
Adams; Long; Johanson
Journal of the American Chemical Society, 1939 , vol. 61, p. 2342,2344
参考文献
Merck
Patent: DE172724 ;
反应条件
1: 99 percent / polyphosphoric acid / 6 h / 120-140 deg C
2: 70 percent / sodium hydroxide / H2O / 24 h / 50 °C
3: 90 percent / tellurium, sodium borohydride, acetic acid / ethanol / Heating; 16-18 h
4: 68 percent / DDQ / benzene / 12 h / Heating
View Scheme
参考文献
Shobana, N.; Yeshoda, P.; Shanmugam, P.
Tetrahedron, 1989 , vol. 45, # 3 p. 757 - 762
参考文献
Baumgarten; Kaergel
Chemische Berichte, 1927 , vol. 60, p. 836