1,3,5-三甲氧基苯合成路线 (共 273 条)
反应条件
n-butyllithium in tetrahydrofuran; hexane; water
参考文献
Warner-Lambertt Company
Patent: US6057315 A1, 2000 ;
反应条件
1: AlCl3 2: aqueous alcoholic potash View Scheme
参考文献
Herzig; Wenzel; Gehringer
Monatshefte fuer Chemie, 1903 , vol. 24, p. 866
反应条件
in neat (no solvent) T=22°C; Irradiation; Rate constant;
参考文献
Shoute, Lian C. T.; Neta, P.
Journal of Physical Chemistry, 1990 , vol. 94, p. 2447 - 2453
反应条件
in cyclohexane T=22°C; Irradiation; Rate constant;
参考文献
Shoute, Lian C. T.; Neta, P.
Journal of Physical Chemistry, 1990 , vol. 94, p. 2447 - 2453
反应条件
trimethylsilyl trifluoromethanesulfonate in 1,2-dichloro-ethane T=24°C; 0.5 h;
参考文献
Chemische Berichte, , vol. 114, # 4 p. 1234 - 1255
反应条件
1: ZnCl2; benzene; HCl / Reaktion des entstandenen Aldimids mit waessr. Salzsaeure 2: pyridine View Scheme
参考文献
Herzig; Wenzel; Gehringer
Monatshefte fuer Chemie, 1903 , vol. 24, p. 866
反应条件
1.1: AlCl3, aluminium chloride / diethyl ether 2.1: bromine; acetic acid / 1 h / 20 °C 3.1: sodium hydroxide / ethanol / 0.08 h 3.2: 20 °C View Scheme
参考文献
Bandgar, Babasaheb P.; Hote, Baliram S.; Dhole, Nagesh A.; Gacche, Rajesh N.
Medicinal Chemistry Research, 2012 , vol. 21, # 9 p. 2292 - 2299
反应条件
1: 85 percent / POCl3 / 40 - 50 °C 2: 82 percent / NH4OAc / Heating 3: LiAlH4 / tetrahydrofuran / 36 h / Heating View Scheme
参考文献
Gallardo-Godoy, Alejandra; Fierro, Angelica; McLean, Thomas H.; Castillo, Mariano; Cassels, Bruce K.; Reyes-Parada, Miguel; Nichols, David E.
Journal of Medicinal Chemistry, 2005 , vol. 48, # 7 p. 2407 - 2419
反应条件
aluminium trichloride; diethyl ether
参考文献
Aghoramurthy et al.
Proceedings - Indian Academy of Sciences, Section A, 1951 , vol. 33, p. 257,261
反应条件
N-bromosuccinmide in tetrachloromethane 3 h; Heating;
参考文献
Mondal, Mukulesh; Puranik, Vedavati G.; Argade, Narshinha P.
Journal of Organic Chemistry, 2006 , vol. 71, # 13 p. 4992 - 4995