1,3,5-三甲氧基苯合成路线 （共 273 条）
反应条件
1: 70 percent / AlCl3 / CH2Cl2 / -10 - -5 °C 2: 38.5 percent / AlCl3 / chlorobenzene / 1 h / Heating View Scheme
参考文献
Gulati; Venkataraman
Journal of the Chemical Society, 1936 , p. 267
反应条件
trifluoroacetic anhydride in dichloromethane T=0°C; 0.166667 h;
参考文献
Fitzpatrick, Leigh; Sala, Tony; Sargent, Melvyn V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 85 - 89
反应条件
2,4-bisbenzyloxy-3-chloro-6-methylbenzoic acid in dichloromethane T=0°C; 0.166667 h;
参考文献
Fitzpatrick, Leigh; Sala, Tony; Sargent, Melvyn V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 85 - 89
反应条件
1: With n-butyllithium in tetrahydrofuran T=0°C; 2 h; Inert atmosphere; 2: With boric acid trimethyl ester in tetrahydrofuran T=-78 - 20°C; Inert atmosphere; 3: With water in tetrahydrofuran T=0°C; 0.5 h;
参考文献
Dennis, Eric G.; Jeffery, David W.; Perkins, Michael V.; Smith, Paul A.
Tetrahedron, 2011 , vol. 67, # 11 p. 2125 - 2131
参考文献
Prey
Chemische Berichte, 1941 , vol. 74, p. 1219,1221
Chemische Berichte, 1942 , vol. 75, p. 350,355, 356, 540
反应条件
in acetonitrile Flash photolysis;
参考文献
Winter, Arthur H.; Gibson, Harry H.; Falvey, Daniel E.
Journal of Organic Chemistry, 2007 , vol. 72, # 22 p. 8186 - 8195
反应条件
in acetonitrile Flash photolysis; Kinetics;
参考文献
Winter, Arthur H.; Gibson, Harry H.; Falvey, Daniel E.
Journal of Organic Chemistry, 2007 , vol. 72, # 22 p. 8186 - 8195
参考文献
Banks,R.E.; Madany,I.M.
Journal of Fluorine Chemistry, 1985 , vol. 30, p. 211
反应条件
nitric acid in acetic acid 1.5 h; Ambient temperature;
参考文献
Sankaraman,S.; Haney,W.A.; Kochi,J.K.
Journal of the American Chemical Society, 1987 , vol. 109, p. 5235
反应条件
1: 96 percent Spectr. / SnCl4 / CH2Cl2 / 20 °C 2: 12 percent / CsOH*H2O / ethane-1,2-diol / 4 h / 160 °C View Scheme
参考文献
Zaltsgendler; Leblanc; Bernstein
Tetrahedron Letters, 1993 , vol. 34, # 15 p. 2441 - 2444
