1,3,5-三甲氧基苯合成路线 （共 273 条）
反应条件
boron trichloride in dichloromethane 20 h; Ambient temperature;
参考文献
Australian Journal of Chemistry, , vol. 38, # 5 p. 777 - 792
反应条件
n-butyllithium; boric acid trimethyl ester; dihydrogen peroxide; acetic acid Yield given. Multistep reaction;
参考文献
Sargent, Melvyn V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 403 - 411
反应条件
3-chloro-benzenecarboperoxoic acid in chloroform Oxidation; 4 h; Heating;
参考文献
Journal of Chemical Research, Miniprint, , # 8 p. 2001 - 2019
反应条件
in acetonitrile Photolysis;
参考文献
Journal of Organic Chemistry, , vol. 72, # 13 p. 4626 - 4634
参考文献
Abramovitch,R.A. et al.
Journal of Organic Chemistry, 1972 , vol. 37, # 17 p. 2705 - 2710
反应条件
1.1: boron trifluoride diethyl etherate / 4 h / 100 °C 1.2: 2 h / |Reflux 2.1: iodine / dimethyl sulfoxide / 4 h / 120 °C View Scheme
参考文献
Liu, Man; Zhang, Ji; Yang, Jian; Yang, Bo; Cui, Wei
Journal of Chemical Research, 2014 , vol. 38, # 3 p. 134 - 136
反应条件
1: With trichlorophosphate T=40°C; Vilsmeier-Haack reaction; 3 h; 2: With 1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione; ammonia in water T=20°C; 3 h; regioselective reaction;
参考文献
Ushijima, Sousuke; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2012 , vol. 68, # 24 p. 4588 - 4595
反应条件
oxygen; copper diacetate; palladium diacetate in dimethyl sulfoxide T=130°C;
参考文献
Yan, Guobing; Kuang, Chunxiang; Zhang, Yan; Wang, Jianbo
Organic Letters, 2010 , vol. 12, # 5 p. 1052 - 1055
反应条件
boron trifluoride diethyl etherate in 1,2-dichloro-ethane T=80°C; 12 h; Sealed vialInert atmosphere; regioselective reaction;
参考文献
Yang, Yang; Zhang, Yan; Wang, Jianbo
Organic Letters, 2011 , vol. 13, # 20 p. 5608 - 5611
反应条件
1: trichlorophosphate / -5 - 0 °C / Inert atmosphere 2: iodine; ammonia / water; tetrahydrofuran / 1 h / 20 °C View Scheme
参考文献
PIRAMAL LIFE SCIENCES LIMITED; BANDGAR, Babasaheb Pandurang; TOTRE, Jalindar Vasant
Patent: WO2011/121505 A1, 2011 ;
