1,3,5-三甲氧基苯合成路线 （共 273 条）
反应条件
palladium diacetate; trifluoroacetic acid
T=20°C; 4 h;
参考文献
Saravanan, Perumal; Anbarasan, Pazhamalai
Organic Letters, 2014 , vol. 16, # 3 p. 848 - 851
反应条件
trifluorormethanesulfonic acid in 1,2-dichloro-ethane
T=100°C; 2 h;
参考文献
Kim, Sundae; Kang, Dongjin; Lee, Chang-Hee; Lee, Phil Ho
Journal of Organic Chemistry, 2012 , vol. 77, # 15 p. 6530 - 6537
反应条件
sodium acetate; acetic acid
参考文献
Meyer,K. H.; Lenhardt
Justus Liebigs Annalen der Chemie, 1913 , vol. 398, p. 69
反应条件
FeCl3·6H2O in dichloromethane
T=0 - 20°C; Friedel Crafts arylation; 2 h; Inert atmosphere;
参考文献
Thirupathi, Ponnaboina; Soo Kim, Sung
Journal of Organic Chemistry, 2010 , vol. 75, # 15 p. 5240 - 5249
反应条件
1: POCl3; diethyl ether / anschliessend Behandeln des Reaktionsprodukts mit wss. NaOH
2: diethyl ether
3: aqueous H2SO4; ethanol
View Scheme
参考文献
Kenyon; Mason
Journal of the Chemical Society, 1952 , p. 4964,4966
参考文献
Lifschitz
Recueil des Travaux Chimiques des Pays-Bas, 1934 , vol. 53, p. 191,194
反应条件
ethyldimethylsilane; (μ3,η2,η3,η5-acenaphthylene)Ru3(CO)7
T=20°C; 5 h; Inert atmosphereNeat (no solvent);
参考文献
Nagashima, Hideo; Kubo, Yuichi; Kawamura, Mitsunobu; Nishikata, Takashi; Motoyama, Yukihiro
Tetrahedron, 2011 , vol. 67, # 40 p. 7667 - 7672
反应条件
1: 1.) n-BuLi / 1.) ether, hexane, reflux, 24 h, 2.) ether, hexane, reflux, 12 h
2: 88 percent / Ph3P, CBr4 / acetonitrile / 2 h / Ambient temperature
3: 1.) Mg, 2.) sat. aq. NH4Cl / 1.) THF, reflux, 3 h
View Scheme
参考文献
Lal, Kasturi; Ghosh, Subrata; Salomon, Robert G.
Journal of Organic Chemistry, 1987 , vol. 52, # 6 p. 1072 - 1078
反应条件
dihydrogen peroxide; sodium chloride in water; acetic acid; 1,2-dichloro-ethane
T=60°C; 2 h; stereoselective reaction;
参考文献
Mizuno, Noritaka; Kamata, Keigo; Yamaguchi, Kazuya
Catalysis Today, 2012 , vol. 185, # 1 p. 157 - 161
反应条件
dihydrogen peroxide; acetic acid; lithium chloride in water; 1,2-dichloro-ethane
T=60°C; 2 h; Inert atmosphere;
参考文献
Yonehara, Kazuhiro; Kamata, Keigo; Yamaguchi, Kazuya; Mizuno, Noritaka
Chemical Communications, 2011 , vol. 47, # 6 p. 1692 - 1694
