1,3,5-三甲氧基苯合成路线 （共 273 条）
反应条件
aluminium trichloride in diethyl ether
4 h;
参考文献
Ahluwalia, Vinod K.; Singh, Daljeet; Singh, Rishi P.
Monatshefte fuer Chemie, 1985 , vol. 116, p. 869 - 872
反应条件
aluminium trichloride
T=100°C; 0.333333 h;
参考文献
Dabbagh, Hossein A.; Noroozi-Pesyan, Nader; Patrick, Brian O.; James, Brian R.
Canadian Journal of Chemistry, 2004 , vol. 82, # 7 p. 1179 - 1185
参考文献
Herzig; Wenzel
Monatshefte fuer Chemie, 1902 , vol. 23, p. 92
反应条件
aluminium trichloride in dichloromethane
T=20°C; 15 h;
参考文献
Helesbeux, Jean-Jacques; Duval, Olivier; Dartiguelongue, Caroline; Seraphin, Denis; Oger, Jean-Michel; Richomme, Pascal
Tetrahedron, 2004 , vol. 60, # 10 p. 2293 - 2300
反应条件
hydrogen fluoride; SbF5
T=-10 - -5°C; 1 h; Yield given. Title compound not separated from byproducts;
参考文献
Repinskaya, I. B.; Barkhutova, D. D.; Makarova, Z. S.; Alekseeva, A. V.; Koptyug, V. A.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, p. 759 - 767
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 4 p. 836 - 845
反应条件
aluminum tri-bromide in nitrobenzene
T=20°C; 24 h;
参考文献
Lee, Yean-Jang; Wu, Tsao-Dong
Journal of the Chinese Chemical Society, 2001 , vol. 48, # 2 p. 201 - 206
反应条件
1: 98 percent / ZnCl2
2: 96 percent / 50 percent aq. KOH / ethanol / 6 h / 20 °C
3: 91 percent / AlCl3 / 10 h / 20 °C
View Scheme
参考文献
Lee, Yean-Jang; Wu, Tsao-Dong
Journal of the Chinese Chemical Society, 2001 , vol. 48, # 2 p. 201 - 206
反应条件
aluminium trichloride in dichloromethane
T=0 - 20°C; 12 h;
参考文献
Mondal, Mukulesh; Puranik, Vedavati G.; Argade, Narshinha P.
Journal of Organic Chemistry, 2007 , vol. 72, # 6 p. 2068 - 2076
反应条件
1: With dimethyl sulfoxide; trifluoroacetic acid; palladium diacetate
T=100°C; 24 h;
2: With water
T=70°C; 2 h;
参考文献
Zhou, Chengxiang; Larock, Richard C.
Journal of Organic Chemistry, 2006 , vol. 71, # 9 p. 3551 - 3558
反应条件
silver trifluoromethanesulfonate in dichloromethane
T=20°C; Friedel-Crafts reaction; 1 h;
参考文献
Yamada, Takeshi; Mishima, Eri; Ueki, Kazuya; Yamago, Shigeru
Chemistry Letters, 2008 , vol. 37, # 6 p. 650 - 651
