1,3,5-三甲氧基苯合成路线 （共 273 条）
反应条件
1: N,N'-tetramethylethylenediamine, nBuLi / hexane
2: diethyl ether / -78 deg C to r.t.
View Scheme
参考文献
Cadamuro, Silvano; Degani, Iacopo; Fochi, Rita; Gatti, Antonella; Regondi, Valeria
Synthesis, 1987 , # 3 p. 311 - 314
反应条件
trifluorormethanesulfonic acid
参考文献
El-Khagawa, Ahmed M.
Bulletin de la Societe Chimique de France, 1987 , # 2 p. 372 - 374
参考文献
Ciamician; Silber
Chemische Berichte, 1894 , vol. 27, p. 1497,1499
反应条件
tetrafluoroboric acid in acetonitrile
T=20°C; 0.666667 h;
参考文献
Dyker, Gerald; Muth, Enrico; Hashmi, A. Stephen K.; Ding, Li
Advanced Synthesis and Catalysis, 2003 , vol. 345, # 11 p. 1247 - 1252
反应条件
gold(III) chloride; silver trifluoromethanesulfonate in 1,2-dichloro-ethane
T=20°C;
参考文献
Li, Zigang; Shi, Zhangjie; He, Chuan
Journal of Organometallic Chemistry, 2005 , vol. 690, # 23 p. 5049 - 5054
反应条件
FeCl3·6H2O in dichloromethane
T=0 - 20°C; Friedel Crafts arylation; 3.5 h; Inert atmosphere;
参考文献
Thirupathi, Ponnaboina; Soo Kim, Sung
Journal of Organic Chemistry, 2010 , vol. 75, # 15 p. 5240 - 5249
反应条件
tin(IV) chloride; di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium
T=90°C; 1 h;
参考文献
Podder, Susmita; Choudhury, Joyanta; Roy, Ujjal Kanti; Roy, Sujit
Journal of Organic Chemistry, 2007 , vol. 72, # 8 p. 3100 - 3103
反应条件
iodine in tetrahydrofuran
T=20°C; aza-Friedel-Crafts reaction;
参考文献
Jaratjaroonphong, Jaray; Krajangsri, Suppachai; Reutrakul, Vichai
Tetrahedron Letters, 2012 , vol. 53, # 19 p. 2476 - 2479
反应条件
iodine in toluene
T=20°C; aza-Friedel-Crafts reaction;
参考文献
Jaratjaroonphong, Jaray; Krajangsri, Suppachai; Reutrakul, Vichai
Tetrahedron Letters, 2012 , vol. 53, # 19 p. 2476 - 2479
反应条件
FeCl3·6H2O in dichloromethane
T=0 - 20°C; Friedel Crafts arylation; 2.5 h; Inert atmosphere;
参考文献
Thirupathi, Ponnaboina; Soo Kim, Sung
Journal of Organic Chemistry, 2010 , vol. 75, # 15 p. 5240 - 5249
