3-羟基-4-甲氧基苯甲醛合成路线 (共 405 条)
反应条件
methanol; amberlyst-15 in toluene T=110°C;
参考文献
Petchmanee, Thaninee; Ploypradith, Poonsakdi; Ruchirawat, Somsak
Journal of Organic Chemistry, 2006 , vol. 71, # 7 p. 2892 - 2895
反应条件
potassium carbonate; isopropyl alcohol; palladium diacetate; triphenylphosphine T=90°C; 14 h;
参考文献
Chen, Jingbo; Zhang, Yushun; Yang, Liquan; Zhang, Xiang; Liu, Jianping; Li, Liang; Zhang, Hongbin
Tetrahedron, 2007 , vol. 63, # 20 p. 4266 - 4270
反应条件
di-isopropyl azodicarboxylate; triphenylphosphine in tetrahydrofuran T=0 - 20°C; Mitsunobu reaction; regioselective reaction;
参考文献
Wang, Xiaolong; Ju, Tingting; Li, Xiaodong; Cao, Xiaoping
Synlett, 2010 , # 19 p. 2947 - 2949
反应条件
sodium methylate; copper dichloride in N,N-dimethyl-formamide T=100 - 105°C; 1.5 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 27, # 7 p. 1380 - 1381
Zhurnal Organicheskoi Khimii, , vol. 27, # 7 p. 1578 - 1579
反应条件
zirconium sulphenyl phosphonate; formyl formic acid T=60°C; 1.5 h;
参考文献
Curini, Massimo; Marcotullio, Maria Carla; Pisani, Emanuela; Rosati, Ornelio; Costantino, Umberto
Synlett, 1997 , vol. 1997, # 7 p. 769 - 770
反应条件
chloro-trimethyl-silane; sodium iodide in water; acetonitrile deprotection; 0.05 h;
参考文献
Kamal, Ahmed; Ramana, K. Venkata; Arifuddin
Chemistry Letters, 1999 , # 8 p. 827 - 828
反应条件
sodium hydroxide in dichloromethane; water T=55 - 60°C; 1.58333 h;
参考文献
Organic Process Research and Development, , vol. 4, # 6 p. 534 - 543
反应条件
AlCl3, aluminium chloride in dichloromethane T=20°C; 5 h;
参考文献
Huang, Wei-Bin; Du, Cai-Yan; Jiang, Jian-An; Ji, Ya-Fei
Research on Chemical Intermediates, 2013 , vol. 39, # 6 p. 2849 - 2856
反应条件
AlCl3, aluminium chloride in dichloromethane T=20°C; 5 h;
参考文献
Huang, Wei-Bin; Du, Cai-Yan; Jiang, Jian-An; Ji, Ya-Fei
Research on Chemical Intermediates, 2013 , vol. 39, # 6 p. 2849 - 2856
反应条件
sodium hydride in dimethyl sulfoxide T=25°C; 17 h; NaH : pyrocatechlol 1.1; Yields of byproduct given;
参考文献
Kessar, Satinder V.; Gupta, Yash P.; Mohammad, Taj; Goyal, Manju; Sawal, Kewal K.
Journal of the Chemical Society, Chemical Communications, 1983 , # 7 p. 400 - 401