3-羟基-4-甲氧基苯甲醛合成路线 （共 405 条）
反应条件
potassium tert-butylate in tetrahydrofuran Horner-Emmons reaction; 2 h; Heating;
参考文献
Lee, Jeewoo; Lee, Jiyoun
Synthetic Communications, 1999 , vol. 29, # 23 p. 4127 - 4140
反应条件
in dichloromethane Wittig reaction; 22 h;
参考文献
Cousin, David; Mann, John; Nieuwenhuyzen, Mark; Van Den Berg, Hendrik
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 1 p. 54 - 62
反应条件
1: With potassium carbonate in toluene 10 h; Reflux; 2: With methanol; sodium tetrahydroborate T=0 - 30°C; 8 h;
参考文献
MSN LABORATORIES LIMITED; SATYANARAYANA REDDY, Manne; THIRUMALAI RAJAN, Srinivasan; ESWARAIAH, Sajja; VENKAT REDDY, Ghojala; RAMA SUBBA REDDY, Karamala; SAHADEVA REDDY, Maramreddy
Patent: WO2011/148392 A1, 2011 ;
Location in patent: Page/Page column 59 ;
反应条件
1: 98 percent / K2CO3 / acetonitrile 2: NaBH4 / ethanol View Scheme
参考文献
MYLAN LABORATORIES LIMITED; RAMA, Shankar; VADALI, Lakshmana Rao; MANUKONDA, Seshadri rao; POTLA, Venkata Srinivas Rao; VADLAMUDI, Mohana Vamsi Krishna; DASARI, Srinivasa Rao
Patent: WO2013/171767 A1, 2013 ;
反应条件
potassium carbonate in acetonitrile 3 h; Reflux;
参考文献
SANOFI-AVENTIS
Patent: US2009/203696 A1, 2009 ;
Location in patent: Page/Page column 20 ;
US 20090203696 A1
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran T=20°C; 20.17 h;
参考文献
VITAE PHARMACEUTICALS, INC.
Patent: WO2007/123718 A1, 2007 ;
Location in patent: Example 1 ;
WO 2007/123718 A1
反应条件
potassium carbonate in acetonitrile
参考文献
Dong, Hua; Zhang, Zhi-Liu; Huang, Jia-Hui; Ma, Rujian; Chen, Shu-Hui; Li, Ge
Tetrahedron Letters, 2005 , vol. 46, # 37 p. 6337 - 6340
反应条件
1: 93 percent / K2CO3 / acetonitrile / 19 h / Heating 2: 72 percent / NaOMe / methanol / 1.5 h / Heating View Scheme
参考文献
Goeschke, Richard; Stutz, Stefan; Heinzelmann, Walter; Maibaum, Juergen
Helvetica Chimica Acta, 2003 , vol. 86, # 8 p. 2848 - 2870
反应条件
bromine; sodium acetate; iron in acetic acid 5 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 5, # 9 p. 1466 - 1471
反应条件
bromine; acetic acid
参考文献
Journal of the Chemical Society, , p. 2279,2287
Journal of Organic Chemistry, , vol. 5, p. 204,208
