3-羟基-4-甲氧基苯甲醛合成路线 (共 405 条)
反应条件
caesium carbonate in N,N-dimethyl-formamide
参考文献
Bioorganic and medicinal chemistry letters, , vol. 12, # 11 p. 1457 - 1461
反应条件
1: potassium carbonate; potassium iodide / ethanol / 10 h / |Reflux 2: trichlorophosphate / 19 h / 100 - 115 °C / |Cooling with ice 3: AlCl3, aluminium chloride / dichloromethane / 5 h / 20 °C View Scheme
参考文献
Research on Chemical Intermediates, , vol. 39, # 6 p. 2849 - 2856
反应条件
hydrogenchloride; water T=170°C;
参考文献
Monatshefte fuer Chemie, , vol. 3, p. 791
Monatshefte fuer Chemie, , vol. 14, p. 383
反应条件
1: MeOH, H2O / acetone 2: 8 mg / 4 h / 150 °C View Scheme
参考文献
Australian Journal of Chemistry, , vol. 42, # 12 p. 2243 - 2263
反应条件
1: 2percent NaOH / H2O / 90 °C 2: conc. HCl / ethanol View Scheme
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 28, # 4 p. 1287 - 1293
反应条件
1: TiCl4 / CH2Cl2 / Ambient temperature 2: conc. aq. HCl / CH2Cl2; diethyl ether / 0.5 h / 0 °C 3: 100 percent / 2N NaOH / Ambient temperature View Scheme
参考文献
Synthetic Communications, , vol. 20, # 17 p. 2565 - 2572
反应条件
1.1: sodium hydroxide; aluminum oxide / water / 0.08 h 1.2: 24 h / 60 °C 2.1: CuCl2·2H2O / ethyl acetate; water / 5 h / 60 °C / |Inert atmosphere 3.1: sodium hydroxide / water; dichloromethane / 1.58 h / 55 - 60 °C View Scheme
参考文献
Organic Process Research and Development, , vol. 4, # 6 p. 534 - 543
反应条件
1: CuCl2·2H2O / ethyl acetate; water / 5 h / 60 °C / |Inert atmosphere 2: sodium hydroxide / water; dichloromethane / 1.58 h / 55 - 60 °C View Scheme
参考文献
Organic Process Research and Development, , vol. 4, # 6 p. 534 - 543
反应条件
in dimethyl sulfoxide T=150°C;
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 28, # 4 p. 1287 - 1293
反应条件
lithium chloride in N,N-dimethyl-formamide 22 h; Heating; Yield given. Yields of byproduct given;
参考文献
Synthesis, , # 4 p. 287 - 289