反应条件
1: 93 percent / CHCl3 / 16 h / Ambient temperature 2: 95 percent / TFAA, pyridine / diethyl ether / 2 h / 0 °C 3: 78 percent / tetrahydrofuran / 1.) -78 deg C, 1 h, 2.) -78 deg C to room temperature, 2 h 4: 56 percent / n-Bu3SnH / tetrahydrofuran / Heating 5: 97 percent / aq. KOH/MeOH / diethyl ether / 12 h View Scheme
参考文献
Osipov, Sergey N.; Golubev, Alexander S.; Sewald, Norbert; Michel, Thomas; Kolomiets, Alexey F.; Fokin, Alexander V.; Burger, Klaus
Journal of Organic Chemistry, 1996 , vol. 61, # 21 p. 7521 - 7528
