4-正丙基-1-庚基-4-醇合成路线 (共 18 条)
反应条件
potassium permanganate; water
参考文献
Schirokow
Journal fuer Praktische Chemie (Leipzig), 1881 , vol. <2>23, p. 201
参考文献
Saizew,P.; Saizew,A.
Justus Liebigs Annalen der Chemie, 1879 , vol. 196, p. 109
反应条件
hydrogen; platinum(IV) oxide; ruthenium in dichloromethane T=20°C; P=760.051 Torr;
参考文献
Organic Letters, , vol. 5, # 4 p. 459 - 462
参考文献
Saizew,P.; Saizew,A.
Justus Liebigs Annalen der Chemie, 1879 , vol. 196, p. 109
反应条件
chromium dichloride in tetrahydrofuran
4.5 h; Ambient temperature;
参考文献
Hiyama, Tamejiro; Okude, Yoshitaka; Kimura, Keizo; Nozaki, Hitosi
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 2 p. 561 - 568
反应条件
hydrogenchloride in diethyl ether
参考文献
Kabi Pharmacia Aktiebolag
Patent: US5155220 A1, 1992 ;
反应条件
4,4'-di-tert-butylbiphenyl; lithium in tetrahydrofuran
T=0°C; 2 h;
参考文献
Yus, Miguel; Martinez, Pedro; Guijarro, David
Synthetic Communications, 2003 , vol. 33, # 13 p. 2365 - 2376
反应条件
heptan-2-one in tetrahydrofuran
T=-78°C; 1 h; further reagent: cyclohexanone; Yield given;
参考文献
Reetz, Manfred T.; Westermann, Juergen; Steinbach, Rainer; Wenderoth, Bernd; Peter, Roland; et al.
Chemische Berichte, 1985 , vol. 118, # 4 p. 1421 - 1440
反应条件
in tetrahydrofuran
4 h;
参考文献
D'Annibale, Andrea; Ciaralli, Laura; Bassetti, Mauro; Pasquini, Chiara
Journal of Organic Chemistry, 2007 , vol. 72, # 16 p. 6067 - 6074
反应条件
phenylpotassium
1.) THF, -40 deg C to 20 deg C, overnight; Yield given. Multistep reaction;
参考文献
Barluenga, Jose; Florez, Josefa; Yus, Miguel
Synthesis, 1985 , # 9 p. 846 - 849