2-(4-甲基苯基)乙酰胺合成路线 (共 6 条)
反应条件
1: With tetrafluoroboric acid; iodobenzene; 3-chloro-benzenecarboperoxoic acid in dichloromethane; water T=25°C; Hofmann rearrangement; 48 h; Inert atmosphere; 2: With hydrogenchloride in dichloromethane; water Inert atmosphere;
参考文献
Miyamoto, Kazunori; Sakai, Yuuta; Goda, Shunsuke; Ochiai, Masahito
Chemical Communications, 2012 , vol. 48, # 7 p. 982 - 984
反应条件
TolSO2N=IPh in dichloromethane T=20°C; Hofmann rearrangement; 1.5 h; Inert atmosphere;
参考文献
Yoshimura, Akira; Luedtke, Matthew W.; Zhdankin, Viktor V.
Journal of Organic Chemistry, 2012 , vol. 77, # 4 p. 2087 - 2091
反应条件
RuCl2(PTA)4; water
T=100°C; 7 h; Green chemistry; Catalytic behavior;
参考文献
Board of Regents of the Nevada System of Higher Education, on behalf of the University of Nevada; Frost, Brian J.; Lee, Wei-Chih
Patent: US2013/96344 A1, 2013 ;
Location in patent: Paragraph 0040; 0041 ;
反应条件
yellow ammonium sulfide
T=250°C; im Druckrohr;
参考文献
Willgerodt
Journal fuer Praktische Chemie (Leipzig), 1909 , vol. <2> 80, p. 189
反应条件
yellow ammonium sulfide
T=250°C;
参考文献
Willgerodt
Journal fuer Praktische Chemie (Leipzig), 1909 , vol. <2> 80, p. 189
Full Text Show Details
Willgerodt
Chemische Berichte, 1888 , vol. 21, p. 534
Journal fuer Praktische Chemie (Leipzig), 1909 , vol. <2> 80, p. 183
Full Text Show Details
Claus; Wehr
Journal fuer Praktische Chemie (Leipzig), 1891 , vol. <2> 44, p. 85
反应条件
1: alcohol
2: H2O2; KOH
View Scheme
参考文献
Radziszewski; Wispek
Chemische Berichte, 1885 , vol. 18, p. 1281
Chemische Berichte, 1882 , vol. 15, p. 1747