3-苯甲酰基-1-甲基吡咯合成路线 （共 9 条）
反应条件
copper ferrite in neat (no solvent)
T=80°C; Friedel-Crafts Acylation; 24 h;
参考文献
Parella, Ramarao; Naveen; Kumar, Amit; Babu, Srinivasarao Arulananda
Tetrahedron Letters, 2013 , vol. 54, # 13 p. 1738 - 1742
反应条件
tetrafluoroboric acid; mercury(II) oxide in tetrahydrofuran
0.5 h; Ambient temperature;
参考文献
Barbero, Margherita; Cadamuro, Silvano; Degani, Iacopo; Fochi, Rita; Gatti, Antonella; Regondi, Valeria
Journal of Organic Chemistry, 1988 , vol. 53, # 10 p. 2245 - 2250
反应条件
1: N-methyl-hydroxylamine hydrochloride; dimethyl acetylenedicarboxylate With potassium hydrogencarbonate in dichloromethane
0.25 h;
2: benzoyl chloride in dichloromethane
T=40°C; 2.5 h;
参考文献
Valizadeh, Hassan; Fakhari, Ashraf
Molecules, 2010 , vol. 15, # 5 p. 2972 - 2979
反应条件
potassium hydroxide in water
10 h; Heating;
参考文献
Chen, Qingqi; Wang, Tianyu; Zhang, Yi; Wang, Qiuan; Ma, Jinshi
Synthetic Communications, 2002 , vol. 32, # 7 p. 1041 - 1049
反应条件
1: 44 percent / pyridine / acetonitrile / 1 h / Ambient temperature
2: 96 percent / HgO, aq. HBF4 / tetrahydrofuran / 0.5 h / Ambient temperature
View Scheme
参考文献
Barbero, Margherita; Cadamuro, Silvano; Degani, Iacopo; Fochi, Rita; Gatti, Antonella; Regondi, Valeria
Journal of Organic Chemistry, 1988 , vol. 53, # 10 p. 2245 - 2250
反应条件
1: 44 percent / pyridine / acetonitrile / 1 h / Ambient temperature
2: 96 percent / HgO, aq. HBF4 / tetrahydrofuran / 0.5 h / Ambient temperature
View Scheme
参考文献
Barbero, Margherita; Cadamuro, Silvano; Degani, Iacopo; Fochi, Rita; Gatti, Antonella; Regondi, Valeria
Journal of Organic Chemistry, 1988 , vol. 53, # 10 p. 2245 - 2250
反应条件
PPA
T=95°C; 2 h; Mechanism;
参考文献
Carson, John R.; Davis, Nancy M.
Journal of Organic Chemistry, 1981 , vol. 46, # 5 p. 839 - 843
反应条件
PPA; sodium acetate; trichlorophosphate
Yield given. Multistep reaction;
参考文献
Carson, John R.; Davis, Nancy M.
Journal of Organic Chemistry, 1981 , vol. 46, # 5 p. 839 - 843
反应条件
sodium acetate; trichlorophosphate
Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Carson, John R.; Davis, Nancy M.
Journal of Organic Chemistry, 1981 , vol. 46, # 5 p. 839 - 843
