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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
62128-44-3
合成路线
(共 8 条)
112816-91-8
→
反应条件
62128-44-3
反应条件
tetrafluoroboric acid; mercury(II) oxide in tetrahydrofuran 0.5 h; Ambient temperature;
参考文献
Barbero, Margherita; Cadamuro, Silvano; Degani, Iacopo; Fochi, Rita; Gatti, Antonella; Regondi, Valeria
Journal of Organic Chemistry, 1988 , vol. 53, # 10 p. 2245 - 2250
4229-44-1
N-甲基羟胺盐酸盐
+
122-01-0
氯化对氯苯甲酰
+
762-42-5
丁炔二酸二甲酯
→
反应条件
62128-44-3
反应条件
1: N-methyl-hydroxylamine hydrochloride; dimethyl acetylenedicarboxylate With potassium hydrogencarbonate in dichloromethane 0.25 h; 2: 4-chloro-benzoyl chloride in dichloromethane T=40°C; 3 h;
参考文献
Valizadeh, Hassan; Fakhari, Ashraf
Molecules, 2010 , vol. 15, # 5 p. 2972 - 2979
62128-32-9
→
反应条件
62128-44-3
反应条件
trifluoroacetic acid T=72°C; 8 h; Heating; Mechanism;
参考文献
Carson, John R.; Davis, Nancy M.
Journal of Organic Chemistry, 1981 , vol. 46, # 5 p. 839 - 843
96-54-8
N-甲基吡咯
→
反应条件
62128-44-3
反应条件
1: 34 percent / pyridine / acetonitrile / 1 h / Ambient temperature 2: 90 percent / HgO, aq. HBF4 / tetrahydrofuran / 0.5 h / Ambient temperature View Scheme
参考文献
Barbero, Margherita; Cadamuro, Silvano; Degani, Iacopo; Fochi, Rita; Gatti, Antonella; Regondi, Valeria
Journal of Organic Chemistry, 1988 , vol. 53, # 10 p. 2245 - 2250
58948-38-2
→
反应条件
62128-44-3
反应条件
1: 34 percent / pyridine / acetonitrile / 1 h / Ambient temperature 2: 90 percent / HgO, aq. HBF4 / tetrahydrofuran / 0.5 h / Ambient temperature View Scheme
参考文献
Barbero, Margherita; Cadamuro, Silvano; Degani, Iacopo; Fochi, Rita; Gatti, Antonella; Regondi, Valeria
Journal of Organic Chemistry, 1988 , vol. 53, # 10 p. 2245 - 2250
76024-67-4
+
100-66-3
苯甲醚
→
反应条件
62128-44-3
+
10547-60-1
4-(4-氯苯甲酰基)苯甲醚
反应条件
PPA T=95°C; 5 h;
参考文献
Carson, John R.; Davis, Nancy M.
Journal of Organic Chemistry, 1981 , vol. 46, # 5 p. 839 - 843
122-01-0
氯化对氯苯甲酰
→
反应条件
62128-44-3
反应条件
1: 100 percent / anhydrous AlCl3 / CH2Cl2 / 0.5 h / Ambient temperature 2: 78 percent / dioxane / 24 h / Ambient temperature View Scheme
参考文献
Cadamuro, Silvano; Degani, Iacopo; Dughera, Stefano; Fochi, Rita; Gatti, Antonella; Piscopo, Laura
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 2 p. 273 - 284
97188-31-3
+
124-41-4
甲醇钠
→
反应条件
62128-38-5
(4-氯苯基)-(1H-吡咯-3-基)甲酮
+
62128-44-3
反应条件
in 1,4-dioxane 24 h; Ambient temperature;
参考文献
Cadamuro, Silvano; Degani, Iacopo; Dughera, Stefano; Fochi, Rita; Gatti, Antonella; Piscopo, Laura
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 2 p. 273 - 284