1,2,3,4-四-O-乙酰基吡喃己醛糖酸合成路线 （共 11 条）
反应条件
triethylamine in acetic anhydride T=100°C; 5 h;
参考文献
Tajima, Kiyohiko
Tetrahedron Letters, 1986 , vol. 27, # 50 p. 6095 - 6098
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in acetic anhydride 16 h; Ambient temperature;
参考文献
Tajima, Kiyohiko
Tetrahedron Letters, 1986 , vol. 27, # 50 p. 6095 - 6098
参考文献
Fry
Journal of the American Chemical Society, 1955 , vol. 77, p. 3915
反应条件
water in tetrahydrofuran
18 h;
参考文献
Ross, Benjamin P.; DeCruz, Shaun E.; Lynch, Thomas B.; Davis-Goff, Karen; Toth, Istvan
Journal of Medicinal Chemistry, 2004 , vol. 47, # 5 p. 1251 - 1258
反应条件
iodine
T=0 - 25°C; Acetylation; 3 h;
参考文献
Malkinson, John P.; Falconer, Robert A.; Toth, Istvan
Journal of Organic Chemistry, 2000 , vol. 65, # 17 p. 5249 - 5252
反应条件
1: iodine / 5 h / 0 - 20 °C
2: water / tetrahydrofuran
View Scheme
参考文献
Granda, Jaroslaw M.; Jurczak, Janusz
Organic Letters, 2013 , vol. 15, # 18 p. 4730 - 4733
反应条件
sodium hydrogencarbonate
参考文献
Fry
Journal of the American Chemical Society, 1955 , vol. 77, p. 3915
反应条件
toluene-4-sulfonic acid
T=0°C; 1.5 h; Title compound not separated from byproducts;
参考文献
Imamura, Takeshi; Watanabe, Takashi; Kuwahara, Masaaki; Koshijima, Tetsuo
Phytochemistry (Elsevier), 1994 , vol. 37, # 4 p. 1165 - 1174
反应条件
1: iodine / 2.5 h / 0 - 20 °C
2: water / tetrahydrofuran / 20 °C
View Scheme
参考文献
El-Nezhawy, Ahmed O.H.; Adly, Frady G.; Eweas, Ahmed F.; Hanna, Atef G.; El-Kholy, Yehya M.; El-Sayed, Shahenaz H.; El-Naggar, Tarek B.A.
Archiv der Pharmazie, 2011 , vol. 344, # 10 p. 648 - 657
反应条件
toluene-4-sulfonic acid
参考文献
Takeda, Yasuko; Akimoto, Toshio; Kyogoku, Yoshimasa
Carbohydrate Research, 1982 , vol. 106, p. 175 - 192
