甲基(2Z)-3-溴丙烯酸酯合成路线 （共 6 条）
反应条件
triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide in tetrahydrofuran Sonogashira coupling-isomerization reaction; 8 h; Heating;
参考文献
Braun, Roland U.; Ansorge, Markus; Mueller, Thomas J. J.
Chemistry - A European Journal, 2006 , vol. 12, # 35 p. 9081 - 9094
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine T=20°C;
参考文献
Bellina; Biagetti; Carpita; Rossi
Tetrahedron, 2001 , vol. 57, # 14 p. 2857 - 2870
反应条件
acetic acid; lithium bromide
T=70°C;
参考文献
Ma, Shengming; Lu, Xiyan; Li, Zhigang
Journal of Organic Chemistry, 1992 , vol. 57, # 2 p. 709 - 713
参考文献
Weir, John R.; Patel, Babu A.; Heck, Richard F.
Journal of Organic Chemistry, 1980 , vol. 45, # 24 p. 4926 - 4931
反应条件
(i) aq. NaHSO4, (ii) SOCl2, (iii) /BRN= 1098229/; Multistep reaction;
参考文献
Holy,A.
Collection of Czechoslovak Chemical Communications, 1974 , vol. 39, p. 3177 - 3186
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium methylate; benzo[1,3,2]dioxaborole
1.) 70 deg C, 1 h, 2.) toluene, 40 deg C, 45 min; rt, overnight; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Baeckstroem, Peter; Jacobsson, Ulla; Norin, Torbjoern; Unelius, C. Rikard
Tetrahedron, 1988 , vol. 44, # 9 p. 2541 - 2548
