反应条件
1: 72 percent / Zn-Cu couple / propan-1-ol / 1.)65 deg C, 2.)80 deg C, 15 min.
2: 1.)methyllithium, diisopropylamine / 1.)ether, HMPA, r.t., 2 h, 2.)ether, -10 deg C, 1 h
3: Bu3SnH / benzene / Heating
View Scheme
参考文献
Apparu, Marcel; Crandall, Jack K.
Journal of Organic Chemistry, 1984 , vol. 49, # 12 p. 2125 - 2130