1,3-二羟基丙酮二聚体合成路线 (共 44 条)
反应条件
acetic acid in water; isopropyl alcohol
参考文献
LG Chem Investment Ltd.
Patent: US6630593 B1, 2003 ;
反应条件
1: With acetic acid in butan-1-ol
T=20°C; 24 h;
2: With water in acetic acid; butan-1-ol
0.5 h;
参考文献
Takeda Chemical Industries, Ltd.
Patent: EP1422228 A1, 2004 ;
Location in patent: Page 232 ;
EP 1422228 A1
参考文献
LG Life Sciences, Ltd.
Patent: US6511978 B1, 2003 ;
US 6511978 B1
反应条件
1: 1,3-dihydroxyacetone dimer With Zn(NO3)2*6H2O; C13H29N5O in 1-methyl-pyrrolidin-2-one; water
T=25°C; 0.166667 h;
2: 4-nitrobenzaldehdye in 1-methyl-pyrrolidin-2-one; water
T=25°C; 42 h;
参考文献
Itoh, Susumu; Kitamura, Masanori; Yamada, Yasuyuki; Aoki, Shin
Chemistry - A European Journal, 2009 , vol. 15, # 40 p. 10570 - 10584