反应条件
1: 1) (COCl)2, DMSO, 2) Et3N / 1) CH2Cl2, -63 deg C, 20 min, 2) -63 deg C, 20 min
2: 1) <V2Cl3(THF)6>2<Zn2Cl6>, 2) 1 M HCl / 1) CH2Cl2, 3 h, 2) 12 h
3: NaH / tetrahydrofuran / 12 h
View Scheme
参考文献
Konradi, Andrei W.; Pedersen, Steven F.
Journal of Organic Chemistry, 1992 , vol. 57, # 1 p. 28 - 32
