(4-甲氧基甲基苯基)甲醇合成路线 (共 15 条)
反应条件
1: 89 percent / SOCl2 / CH2Cl2 2: 91 percent / HNO3 / CH2Cl2 / 1 h / 20 °C View Scheme
参考文献
Strazzolini, Paolo; Runcio, Antonio
European Journal of Organic Chemistry, 2003 , # 3 p. 526 - 536
反应条件
nitric acid in dichloromethane T=20°C; 1 h;
参考文献
European Journal of Organic Chemistry, , # 3 p. 526 - 536
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Strazzolini, Paolo; Runcio, Antonio
European Journal of Organic Chemistry, 2003 , # 3 p. 526 - 536
反应条件
hydrogen; Pt1Ru5; silica gel in ethanol
T=99.85°C; P=15001.2 Torr; 8 h; Product distribution; Further Variations:Catalystsreaction times;
参考文献
Raja, Robert; Khimyak, Tetyana; Thomas, John Meurig; Hermans, Sophie; Johnson, Brian F. G.
Angewandte Chemie - International Edition, 2001 , vol. 40, # 24 p. 4638 - 4642
反应条件
sodium hydride in tetrahydrofuran
T=20°C;
参考文献
Zheng, Qi-Huang; Liu, Xuan; Fei, Xiangshu; Wang, Ji-Quan; Ohannesian, David W.; Erickson, Leonard C.; Stone, K. Lee; Martinez, Tanya D.; Miller, Kathy D.; Hutchins, Gary D.
Journal of Labelled Compounds and Radiopharmaceuticals, 2002 , vol. 45, # 14 p. 1239 - 1252
反应条件
1: 87 percent / SOCl2 / 4 h / -30 - 20 °C
2: 94 percent / LiAlH4 / diethyl ether
View Scheme
参考文献
Strazzolini, Paolo; Runcio, Antonio
European Journal of Organic Chemistry, 2003 , # 3 p. 526 - 536
反应条件
1: 91 percent / HNO3 / CH2Cl2 / 1 h / 20 °C
2: 87 percent / SOCl2 / 4 h / -30 - 20 °C
3: 94 percent / LiAlH4 / diethyl ether
View Scheme
参考文献
Strazzolini, Paolo; Runcio, Antonio
European Journal of Organic Chemistry, 2003 , # 3 p. 526 - 536
反应条件
sodium carbonate
T=150°C;
参考文献
Quelet
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1931 , vol. 192, p. 1391,1392
Bulletin de la Societe Chimique de France, 1933 , vol. <4> 53, p. 222,231
反应条件
aluminum oxide in cyclohexane
2 h; Heating; Yield given. Yields of byproduct given;
参考文献
Ogawa, Haruo; Ichimura, Youko; Chihara, Teiji; Teratani, Shousuke; Taya, Kazuo
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, # 8 p. 2481 - 2484
参考文献
Quelet
Bulletin de la Societe Chimique de France, 1933 , vol. <4> 53, p. 222,233