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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
62195-05-5
合成路线
（共 10 条）
62195-32-8
→
反应条件
62195-05-5
反应条件
trichlorophosphate T=115°C; 1 h;
参考文献
Arias, Lucina; Salgado-Zamora, Hector; Cervantes, Humberto; Campos, Elena; Reyes, Alicia; Taylor, Edward C.
Journal of Heterocyclic Chemistry, 2006 , vol. 43, # 3 p. 565 - 569
→
反应条件
62195-05-5
反应条件
in 1-methyl-pyrrolidin-2-one T=170°C; 96 h; Sealed tube;
参考文献
Bazin, Marc-Antoine; Marhadour, Sophie; Tonnerre, Alain; Marchand, Pascal
Tetrahedron Letters, 2013 , vol. 54, # 39 p. 5378 - 5382
504-29-0
2-氨基吡啶
→
反应条件
62195-05-5
反应条件
1.1: ethylene glycol dimethyl ether / 20 °C 1.2: Heating 2.1: sulfuric acid; nitric acid / 0 - 5 °C 3.1: ammonium hydroxide / 8 h / 20 °C 4.1: trichlorophosphate / 1 h / 110 °C View Scheme
参考文献
Lopez-Martinez, Margarita; Salgado-Zamora, Hector; Campos-Aldrete, Ma. Elena; Trujillo-Ferrara, Jose G.; Correa-Basurto, Jose; Mexica-Ochoa, Carlos
Medicinal Chemistry Research, 2012 , vol. 21, # 4 p. 415 - 420
126202-06-0
(2-氨基-1-吡啶鎓基)乙酸酯
→
反应条件
62195-05-5
反应条件
1: trichlorophosphate / toluene / 16 h / |Reflux 2: sulfuric acid; nitric acid / 3.5 h / -5 - 20 °C 3: 1-methyl-pyrrolidin-2-one / 96 h / 170 °C / |Sealed tube View Scheme
参考文献
Bazin, Marc-Antoine; Marhadour, Sophie; Tonnerre, Alain; Marchand, Pascal
Tetrahedron Letters, 2013 , vol. 54, # 39 p. 5378 - 5382
3999-05-1
→
反应条件
62195-05-5
反应条件
1: sulfuric acid; nitric acid / 3.5 h / -5 - 20 °C 2: 1-methyl-pyrrolidin-2-one / 96 h / 170 °C / |Sealed tube View Scheme
参考文献
Bazin, Marc-Antoine; Marhadour, Sophie; Tonnerre, Alain; Marchand, Pascal
Tetrahedron Letters, 2013 , vol. 54, # 39 p. 5378 - 5382
38922-77-9
咪唑吡啶-2-羧酸乙酯
→
反应条件
62195-05-5
反应条件
1: sulfuric acid; nitric acid / 0 - 5 °C 2: ammonium hydroxide / 8 h / 20 °C 3: trichlorophosphate / 1 h / 110 °C View Scheme
参考文献
Lopez-Martinez, Margarita; Salgado-Zamora, Hector; Campos-Aldrete, Ma. Elena; Trujillo-Ferrara, Jose G.; Correa-Basurto, Jose; Mexica-Ochoa, Carlos
Medicinal Chemistry Research, 2012 , vol. 21, # 4 p. 415 - 420
62223-44-3
→
反应条件
62195-05-5
反应条件
1: ammonium hydroxide / 8 h / 20 °C 2: trichlorophosphate / 1 h / 110 °C View Scheme
参考文献
Lopez-Martinez, Margarita; Salgado-Zamora, Hector; Campos-Aldrete, Ma. Elena; Trujillo-Ferrara, Jose G.; Correa-Basurto, Jose; Mexica-Ochoa, Carlos
Medicinal Chemistry Research, 2012 , vol. 21, # 4 p. 415 - 420
64-17-5
乙醇
+
62195-05-5
→
反应条件
89717-70-4
反应条件
sodium ethanolate T=60°C; 2 h;
参考文献
Arias, Lucina; Salgado-Zamora, Hector; Cervantes, Humberto; Campos, Elena; Reyes, Alicia; Taylor, Edward C.
Journal of Heterocyclic Chemistry, 2006 , vol. 43, # 3 p. 565 - 569
141-43-5
乙醇胺
+
62195-05-5
→
反应条件
62194-92-7
反应条件
lithium hydroxide T=70°C; 1 h;
参考文献
Hernandez, Jorge; Salgado-Zamora, Hector; Cervantes, Humberto; Arias, Lucina; Campos, Ma. Elena
Heterocyclic Communications, 2009 , vol. 15, # 1 p. 73 - 78
56-40-6
甘氨酸
+
62195-05-5
→
反应条件
62194-95-0
反应条件
sodium hydrogencarbonate in N,N-dimethyl-formamide T=130 - 132°C; 25 h; Inert atmosphere;
参考文献
Hernandez, Jorge; Salgado-Zamora, Hector; Cervantes, Humberto; Arias, Lucina; Campos, Ma. Elena
Heterocyclic Communications, 2009 , vol. 15, # 1 p. 73 - 78
