2-氯-5-异氰酸硝基苯合成路线 (共 152 条)
反应条件
in methanol
0.5 h; Ambient temperature; Mechanism;
参考文献
Naddaka, V. I.; Avanesyan, K. V.; Cherkinskaya, M. L.; Minkin, V. I.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 12 p. 2245 - 2250
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 12 p. 2489 - 2494
反应条件
1: 1.55 h / -261.16 °C / Ar matrix photolysis
2: 3.67 h / -261.16 °C / Ar matrix photolysis
View Scheme
参考文献
Begue, Didier; Qiao, Greg Guanghua; Wentrup, Curt
Journal of the American Chemical Society, 2012 , vol. 134, # 11 p. 5339 - 5350
参考文献
Richter, Frank U.
Chemistry - A European Journal, 2009 , vol. 15, # 21 p. 5200 - 5202
反应条件
in diethyl ether; ethanol; 2-methyl-butane
T=-193.1°C; Irradiation;
参考文献
Csongar, Christian; Leihkauf, Peter; Lohse, Volkmar; Tomaschewski, Georg
Zeitschrift fuer Chemie (Stuttgart, Germany), 1984 , vol. 24, # 3 p. 96 - 97
反应条件
in tetrachloromethane
T=80°C; 0.5 h; other time, other molar ratio, study of IR spectra of reaction mixture; Product distribution;
参考文献
Bakhitov, M. I.; Zharkov, V. V.; Kuznetsov, E. V.; Khazeeva, Z. Kh.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 3 p. 552 - 555,432 - 435
反应条件
in toluene
24 h; Heating; Product distribution; Further Variations:Temperaturestime;
参考文献
Ghosh, Rajshekhar; Samuelson, Ashoka G.
Chemical Communications, 2005 , # 15 p. 2017 - 2019
参考文献
Werner
Journal of the Chemical Society, 1890 , vol. 57, p. 303
参考文献
Stolle
Chemische Berichte, 1908 , vol. 41, p. 1126
反应条件
T=180°C; im Druckrohr;
参考文献
Stolle
Chemische Berichte, 1908 , vol. 41, p. 1126
反应条件
bei der Destillation;
参考文献
Weith
Chemische Berichte, 1874 , vol. 7, p. 1308