2-氯-5-异氰酸硝基苯合成路线 (共 152 条)
反应条件
methyl phosphorodichloridite; triethylamine in diethyl ether
参考文献
Nikonorov, K. V.; Gurylev, E. A.; Antokhina, L. A.; Latypov, Z. Ya.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 12 p. 2330 - 2333
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 12 p. 2796 - 2800
反应条件
in benzene
2 h; Heating;
参考文献
Barbaro, Gaetano; Battaglia, Arturo; Giorgianni, Patrizia; Guerrini, Andrea; Seconi, Giancarlo
Journal of Organic Chemistry, 1995 , vol. 60, # 19 p. 6032 - 6039
反应条件
1: phenyl isocyanate With DMPO in 1-methyl-pyrrolidin-2-one
0.0833333 h;
2: 2,6-Bis(1-methylethyl)phenyl isocyanate in 1-methyl-pyrrolidin-2-one
参考文献
Chen, An-Liu; Wei, Kuan-Liang; Jeng, Ru-Jong; Lin, Jiang-Jen; Dai, Shenghong A.
Macromolecules, 2011 , vol. 44, # 1 p. 46 - 59
反应条件
in benzene
5 h; Ambient temperature;
参考文献
Boedeker, J.; Courault, K.; Koeckritz, A.; Koeckritz, P.
Journal fuer Praktische Chemie (Leipzig), 1983 , vol. 325, # 3 p. 463 - 474
反应条件
aluminum oxide; LutClO4
constant current electrolysis;
参考文献
Ohmori, Hidenobu; Sakai, Kiyoshi; Nagai, Noriko; Mizuki, Yasuyuki; Masui, Masaichiro
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 1 p. 373 - 376
反应条件
in tetrahydrofuran; diethyl ether
added at -10 deg C, then 15 min at 20 deg C;
参考文献
Kolodyazhnyi, O. I.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 6 p. 1314 - 1318,1156 - 1159
反应条件
1: in toluene
T=110°C;
2: With water
参考文献
Kumar, Akshai; Samuelson, Ashoka G
Journal of Chemical Sciences, 2012 , vol. 124, # 6 p. 1343 - 1352
反应条件
1: in toluene
T=110°C;
2: With water
参考文献
Kumar, Akshai; Samuelson, Ashoka G
Journal of Chemical Sciences, 2012 , vol. 124, # 6 p. 1343 - 1352
反应条件
1: in toluene
T=110°C;
2: With water
参考文献
Kumar, Akshai; Samuelson, Ashoka G
Journal of Chemical Sciences, 2012 , vol. 124, # 6 p. 1343 - 1352
反应条件
1: in toluene
T=110°C;
2: With water
参考文献
Kumar, Akshai; Samuelson, Ashoka G
Journal of Chemical Sciences, 2012 , vol. 124, # 6 p. 1343 - 1352